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Continuous operation characteristics of chemical looping hydrogen production system

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  • Cho, Won Chul
  • Lee, Do Yeon
  • Seo, Myung Won
  • Kim, Sang Done
  • Kang, KyoungSoo
  • Bae, Ki Kwang
  • Kim, Change Hee
  • Jeong, SeongUk
  • Park, Chu Sik

Abstract

Three-reactor chemical looping (TRCL) is a hydrogen and electricity production technology with inherent separation of carbon dioxide by use of the iron-based oxygen carrier particles. In this study, an integrated continuous operation test unit (300Wth) using 20wt% Fe2O3/ZrO2as an oxygen carrier was successfully operated over 13h. The average CH4 conversion was 94.15% in a fuel reactor in a moving bed mode. Nearly pure hydrogen (99.95%) was obtained from a steam reactor (SR). The steam conversion to H2 was around 63% of the thermodynamic limit in the SR. The hydrogen containing CO was observed from the SR when the carbon deposited particles were introduced into the SR. During the continuous operation, the oxygen carrier particles maintained its physical and chemical properties with high durability in the TRCL system.

Suggested Citation

  • Cho, Won Chul & Lee, Do Yeon & Seo, Myung Won & Kim, Sang Done & Kang, KyoungSoo & Bae, Ki Kwang & Kim, Change Hee & Jeong, SeongUk & Park, Chu Sik, 2014. "Continuous operation characteristics of chemical looping hydrogen production system," Applied Energy, Elsevier, vol. 113(C), pages 1667-1674.
    • Handle: RePEc:eee:appene:v:113:y:2014:i:c:p:1667-1674
    DOI: 10.1016/j.apenergy.2013.08.078
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    1. Luo, Ming & Yi, Yang & Wang, Shuzhong & Wang, Zhuliang & Du, Min & Pan, Jianfeng & Wang, Qian, 2018. "Review of hydrogen production using chemical-looping technology," Renewable and Sustainable Energy Reviews, Elsevier, vol. 81(P2), pages 3186-3214.
    2. Zhu, Min & Chen, Shiyi & Soomro, Ahsanullah & Hu, Jun & Sun, Zhao & Ma, Shiwei & Xiang, Wenguo, 2018. "Effects of supports on reduction activity and carbon deposition of iron oxide for methane chemical looping hydrogen generation," Applied Energy, Elsevier, vol. 225(C), pages 912-921.
    3. Zhang, Shuai & Xiao, Rui & Zheng, Wenguang, 2014. "Comparative study between fluidized-bed and fixed-bed operation modes in pressurized chemical looping combustion of coal," Applied Energy, Elsevier, vol. 130(C), pages 181-189.
    4. Voitic, Gernot & Nestl, Stephan & Lammer, Michael & Wagner, Julian & Hacker, Viktor, 2015. "Pressurized hydrogen production by fixed-bed chemical looping," Applied Energy, Elsevier, vol. 157(C), pages 399-407.
    5. Esteban-Díez, G. & Gil, María V. & Pevida, C. & Chen, D. & Rubiera, F., 2016. "Effect of operating conditions on the sorption enhanced steam reforming of blends of acetic acid and acetone as bio-oil model compounds," Applied Energy, Elsevier, vol. 177(C), pages 579-590.
    6. Khan, Mohammed N. & Shamim, Tariq, 2016. "Investigation of hydrogen generation in a three reactor chemical looping reforming process," Applied Energy, Elsevier, vol. 162(C), pages 1186-1194.
    7. Hua, Xiuning & Fan, Yiran & Wang, Yidi & Fu, Tiantian & Fowler, G.D. & Zhao, Dongmei & Wang, Wei, 2017. "The behaviour of multiple reaction fronts during iron (III) oxide reduction in a non-steady state packed bed for chemical looping water splitting," Applied Energy, Elsevier, vol. 193(C), pages 96-111.
    8. Cho, Won Chul & Lee, Jun Kyu & Nam, Gyeong Duk & Kim, Chang Hee & Cho, Hyun-Seok & Joo, Jong Hoon, 2019. "Degradation analysis of mixed ionic-electronic conductor-supported iron-oxide oxygen carriers for chemical-looping conversion of methane," Applied Energy, Elsevier, vol. 239(C), pages 644-657.
    9. Sun, Zhao & Chen, Shiyi & Hu, Jun & Chen, Aimin & Rony, Asif Hasan & Russell, Christopher K. & Xiang, Wenguo & Fan, Maohong & Darby Dyar, M. & Dklute, Elizabeth C., 2018. "Ca2Fe2O5: A promising oxygen carrier for CO/CH4 conversion and almost-pure H2 production with inherent CO2 capture over a two-step chemical looping hydrogen generation process," Applied Energy, Elsevier, vol. 211(C), pages 431-442.
    10. García-Díez, E. & García-Labiano, F. & de Diego, L.F. & Abad, A. & Gayán, P. & Adánez, J. & Ruíz, J.A.C., 2016. "Optimization of hydrogen production with CO2 capture by autothermal chemical-looping reforming using different bioethanol purities," Applied Energy, Elsevier, vol. 169(C), pages 491-498.
    11. Medrano, J.A. & Hamers, H.P. & Williams, G. & van Sint Annaland, M. & Gallucci, F., 2015. "NiO/CaAl2O4 as active oxygen carrier for low temperature chemical looping applications," Applied Energy, Elsevier, vol. 158(C), pages 86-96.

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