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Preparation of various hierarchical HZSM-5 based catalysts for in-situ fast upgrading of bio-oil

Author

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  • Chaihad, Nichaboon
  • Situmorang, Yohanes Andre
  • Anniwaer, Aisikaer
  • Kurnia, Irwan
  • Karnjanakom, Surachai
  • Kasai, Yutaka
  • Abudula, Abuliti
  • Reubroycharoen, Prasert
  • Guan, Guoqing

Abstract

Hierarchical HZSM-5 zeolites were prepared by desilication of commercial HZSM-5 in aqueous NaOH solutions with the assistance of tetrapropylammonium hydroxides (TPAOH), and applied for the catalytic upgrading of bio-oil derived from the fast pyrolysis of sunflower stalk. The hierarchical HZSM-5 by using 0.2 M NaOH with 0.25 M TPAOH for the desilication exhibited the best catalytic performance and the relative total peak area related to the aromatic hydrocarbons reached 65.8% with a yield of the detected aromatic hydrocarbons up to 45.2 mg/g-bio-oil. With the assistance of 0.25 M TPAOH for the desilication, the formation of mesopores became highly controllable, resulting in the increase in the surface area and maintainment of enough acid amounts, however, the coking on the surface of catalyst was not hindered. To solve the coking problem and increase the aromatic hydrocarbons production, the hierarchical HZSM-5 with the best performance was modified by various metals. It is found that 0.25 wt% Cu loaded hierarchical HZSM-5 increased the yield of the detected aromatic hydrocarbons up to 54.5 mg/g-bio-oil with a decrease in the coke formation.

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  • Chaihad, Nichaboon & Situmorang, Yohanes Andre & Anniwaer, Aisikaer & Kurnia, Irwan & Karnjanakom, Surachai & Kasai, Yutaka & Abudula, Abuliti & Reubroycharoen, Prasert & Guan, Guoqing, 2021. "Preparation of various hierarchical HZSM-5 based catalysts for in-situ fast upgrading of bio-oil," Renewable Energy, Elsevier, vol. 169(C), pages 283-292.
    • Handle: RePEc:eee:renene:v:169:y:2021:i:c:p:283-292
    DOI: 10.1016/j.renene.2021.01.013
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    References listed on IDEAS

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    1. Palizdar, A. & Sadrameli, S.M., 2020. "Catalytic upgrading of biomass pyrolysis oil over tailored hierarchical MFI zeolite: Effect of porosity enhancement and porosity-acidity interaction on deoxygenation reactions," Renewable Energy, Elsevier, vol. 148(C), pages 674-688.
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    Cited by:

    1. Zhang, Qiaofei & Han, Qi & Bai, Hongjuan & Li, Yakun & Zhu, Chunshan & Xie, Wenlei, 2024. "Monolithic HZSM-5/SS-fiber catalysts with high coke-resistance and selectivity for catalytic cracking of castor oil to produce biofuel," Renewable Energy, Elsevier, vol. 229(C).
    2. Chaerusani, Virdi & Ramli, Yusrin & Zahra, Aghietyas Choirun Az & Zhang, Pan & Rizkiana, Jenny & Kongparakul, Suwadee & Samart, Chanatip & Karnjanakom, Surachai & Kang, Dong-Jin & Abudula, Abuliti & G, 2024. "In-situ catalytic upgrading of bio-oils from rapid pyrolysis of torrefied giant miscanthus (Miscanthus x giganteus) over copper‑magnesium bimetal modified HZSM-5," Applied Energy, Elsevier, vol. 353(PA).
    3. Douvartzides, Savvas & Charisiou, Nikolaos D. & Wang, Wen & Papadakis, Vagelis G. & Polychronopoulou, Kyriaki & Goula, Maria A., 2022. "Catalytic fast pyrolysis of agricultural residues and dedicated energy crops for the production of high energy density transportation biofuels. Part II: Catalytic research," Renewable Energy, Elsevier, vol. 189(C), pages 315-338.

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