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Preparation and performance investigation of a lignin-based solid acid catalyst manufactured from olive cake for biodiesel production

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  • Sandouqa, Arwa
  • Al-Hamamre, Zayed
  • Asfar, Jamil

Abstract

In this study, the olive cake was successfully developed and applied as a substrate to produce a lignin-based catalyst for biodiesel production. Three lignin-based solid acid catalysts were prepared from the incomplete carbonized alkali lignin using concentrated sulfuric acid. The catalyst underwent a detailed characterization analysis in terms of its functional groups of active sites, surface area, acid sites density and morphological structure. For the catalytic activity test, prepared catalysts were studied for their ability to catalyze both esterification and transesterification reactions of waste vegetable oil (WVO) ≈2 FFA (% w/w).

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  • Sandouqa, Arwa & Al-Hamamre, Zayed & Asfar, Jamil, 2019. "Preparation and performance investigation of a lignin-based solid acid catalyst manufactured from olive cake for biodiesel production," Renewable Energy, Elsevier, vol. 132(C), pages 667-682.
    • Handle: RePEc:eee:renene:v:132:y:2019:i:c:p:667-682
    DOI: 10.1016/j.renene.2018.08.029
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    3. Zhang, Bingxin & Gao, Ming & Tang, Weiqi & Wang, Xiaona & Wu, Chuanfu & Wang, Qunhui & Cheung, Siu Ming & Chen, Xiankun, 2023. "Esterification efficiency improvement of carbon-based solid acid catalysts induced by biomass pretreatments: Intrinsic mechanism," Energy, Elsevier, vol. 263(PB).
    4. Mohammad Alnaief & Arwa Sandouqa & Ibrahem Altarawneh & Mohammad Al-Shannag & Malek Alkasrawi & Zayed Al-hamamre, 2020. "Adsorption Characteristics and Potential of Olive Cake Alkali Residues for Biodiesel Purification," Energies, MDPI, vol. 14(1), pages 1-12, December.
    5. Sandouqa, Arwa & Al-Shannag, Mohammad & Al-Hamamre, Zayed, 2020. "Biodiesel purification using biomass-based adsorbent manufactured from delignified olive cake residues," Renewable Energy, Elsevier, vol. 151(C), pages 103-117.
    6. Rokhum, Samuel Lalthazuala & Changmai, Bishwajit & Kress, Thomas & Wheatley, Andrew E.H., 2022. "A one-pot route to tunable sugar-derived sulfonated carbon catalysts for sustainable production of biodiesel by fatty acid esterification," Renewable Energy, Elsevier, vol. 184(C), pages 908-919.
    7. Al-Hamamre, Zayed & Sandouqa, Arwa & Al-Saida, Basel & Shawabkeh, Reyad A. & Alnaief, Mohammad, 2023. "Biodiesel production from waste cooking oil using heterogeneous KNO3/Oil shale ash catalyst," Renewable Energy, Elsevier, vol. 211(C), pages 470-483.
    8. Zailan, Zarifah & Tahir, Muhammad & Jusoh, Mazura & Zakaria, Zaki Yamani, 2021. "A review of sulfonic group bearing porous carbon catalyst for biodiesel production," Renewable Energy, Elsevier, vol. 175(C), pages 430-452.
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    10. Che Zhao & Hongyuan Chen & Xiao Wu & Rui Shan, 2023. "Exploiting the Waste Biomass of Durian Shell as a Heterogeneous Catalyst for Biodiesel Production at Room Temperature," IJERPH, MDPI, vol. 20(3), pages 1-10, January.
    11. Gualberto Zavarize, Danilo & Braun, Heder & Diniz de Oliveira, Jorge, 2021. "Methanolysis of low-FFA waste cooking oil with novel carbon-based heterogeneous acid catalyst derived from Amazon açaí berry seeds," Renewable Energy, Elsevier, vol. 171(C), pages 621-634.
    12. Paritosh, Kunwar & Bose, Archishman, 2024. "Application of biogenic carbon in renewable energy vectors and devices: A step forward to decarbonization," Renewable and Sustainable Energy Reviews, Elsevier, vol. 197(C).
    13. Leesing, Ratanaporn & Siwina, Siraprapha & Fiala, Khanittha, 2021. "Yeast-based biodiesel production using sulfonated carbon-based solid acid catalyst by an integrated biorefinery of durian peel waste," Renewable Energy, Elsevier, vol. 171(C), pages 647-657.
    14. Aisien, Felix Aibuedefe & Aisien, Eki Tina, 2023. "Modeling and optimization of transesterification of rubber seed oil using sulfonated CaO derived from giant African land snail (Achatina fulica) catalyst by response surface methodology," Renewable Energy, Elsevier, vol. 207(C), pages 137-146.
    15. Zhang, Qiaofei & Xie, Wenlei & Li, Jiangbo & Guo, Lihong, 2023. "Bimetallic Zrx-Aly-KIT-6 modified with sulfate as acidic catalyst for biodiesel production from low-grade acidic oils," Renewable Energy, Elsevier, vol. 217(C).
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