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Structural analysis of bio-oils from sub-and supercritical water liquefaction of woody biomass

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  • Qian, Yejian
  • Zuo, Chengji
  • Tan, Jian
  • He, Jianhui

Abstract

Woody biomass was liquefied by water in an autoclave in the reaction temperature range of 280–420°C with sodium carbonate as the catalyst. The experimental results show that the yield of the main liquefaction product (heavy oil) was significantly influenced by the process conditions. The maximum yield of heavy oil was obtained at reaction temperature 380°C. The heavy oils obtained at different reaction temperature were analyzed by Fourier transform infrared spectroscopy (FTIR) and gas chromatography/mass spectrometry (GC/MS). The analytical results show the heavy oil is complex compound that contain hydrocarbon, aldehyde, ketone, hydroxybenzene and ester.

Suggested Citation

  • Qian, Yejian & Zuo, Chengji & Tan, Jian & He, Jianhui, 2007. "Structural analysis of bio-oils from sub-and supercritical water liquefaction of woody biomass," Energy, Elsevier, vol. 32(3), pages 196-202.
    • Handle: RePEc:eee:energy:v:32:y:2007:i:3:p:196-202
    DOI: 10.1016/j.energy.2006.03.027
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    References listed on IDEAS

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    15. Shui, Hengfu & Shan, Chuanjun & Cai, Zhengyi & Wang, Zhicai & Lei, Zhiping & Ren, Shibiao & Pan, Chunxiu & Li, Haiping, 2011. "Co-liquefaction behavior of a sub-bituminous coal and sawdust," Energy, Elsevier, vol. 36(11), pages 6645-6650.
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    17. Yuan, X.Z. & Li, H. & Zeng, G.M. & Tong, J.Y. & Xie, W., 2007. "Sub- and supercritical liquefaction of rice straw in the presence of ethanol–water and 2-propanol–water mixture," Energy, Elsevier, vol. 32(11), pages 2081-2088.
    18. Sun, Peiqin & Heng, Mingxing & Sun, Shaohui & Chen, Junwu, 2010. "Direct liquefaction of paulownia in hot compressed water: Influence of catalysts," Energy, Elsevier, vol. 35(12), pages 5421-5429.
    19. Shuping, Zou & Yulong, Wu & Mingde, Yang & Kaleem, Imdad & Chun, Li & Tong, Junmao, 2010. "Production and characterization of bio-oil from hydrothermal liquefaction of microalgae Dunaliella tertiolecta cake," Energy, Elsevier, vol. 35(12), pages 5406-5411.
    20. Yuan, Xingzhong & Wang, Jingyu & Zeng, Guangming & Huang, Huajun & Pei, Xiaokai & Li, Hui & Liu, Zhifeng & Cong, Minghui, 2011. "Comparative studies of thermochemical liquefaction characteristics of microalgae using different organic solvents," Energy, Elsevier, vol. 36(11), pages 6406-6412.
    21. Leng, Lijian & Yuan, Xingzhong & Chen, Xiaohong & Huang, Huajun & Wang, Hou & Li, Hui & Zhu, Ren & Li, Shanxing & Zeng, Guangming, 2015. "Characterization of liquefaction bio-oil from sewage sludge and its solubilization in diesel microemulsion," Energy, Elsevier, vol. 82(C), pages 218-228.
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    23. Li, Wei-Gang & Zhao, Wei & Liu, Hao-Miao & Ao, Lei & Liu, Kai-Shuai & Guan, Yin-Shuang & Zai, Shi-Feng & Chen, Shang-Long & Zong, Zhi-Min & Wei, Xian-Yong, 2018. "Supercritical ethanolysis of wheat stalk over calcium oxide," Renewable Energy, Elsevier, vol. 120(C), pages 300-305.
    24. Medrano, J.A. & Oliva, M. & Ruiz, J. & García, L. & Arauzo, J., 2011. "Hydrogen from aqueous fraction of biomass pyrolysis liquids by catalytic steam reforming in fluidized bed," Energy, Elsevier, vol. 36(4), pages 2215-2224.
    25. Zhu, Guangyong & Zhu, Xian & Fan, Qi & Wan, Xueliang, 2011. "Recovery of biomass wastes by hydrolysis in sub-critical water," Resources, Conservation & Recycling, Elsevier, vol. 55(4), pages 409-416.

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