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Development of a lithium based chicken bone (Li-Cb) composite as an efficient catalyst for biodiesel production

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  • AlSharifi, Mariam
  • Znad, Hussein

Abstract

A lithium based chicken bone (Li-Cb) composite has been synthesized by wet impregnation method followed by calcination at various temperatures (750, 800, 850, and 900 °C). The Li-Cb catalysts were characterized by Field Emission Scanning Electron Microscope (FESEM), Brunauer–Emmett–Teller surface area (BET), X-ray diffraction (XRD), TG-DSC and Fourier-transform infrared spectroscopy (FT-IR). The catalytic activities of Li impregnated catalyst were described in term of basicity. 2 g of LiNO3 impregnated in 7 g of Cb and calcinated at 850 °C (2Li-Cb850) were found as the best combination to synthesize the efficient catalyst for the transesterification of canola oil with 96.6% conversion to FAME in 3 h of reaction time along with 18:1 of methanol:oil molar ratio, catalyst loading of 4 wt %, and reaction temperature of 60 °C. The pseudo-first order model with 0.58 h−1 rate constant (at 60 °C) and 16.9 kJ/mol activation energy was the best fitted to represent the transesterification kinetic. Moreover, the prepared catalyst (2Li-Cb850) showed sustained activity after being recycled and reused for 5 times with FAME content > 82%.

Suggested Citation

  • AlSharifi, Mariam & Znad, Hussein, 2019. "Development of a lithium based chicken bone (Li-Cb) composite as an efficient catalyst for biodiesel production," Renewable Energy, Elsevier, vol. 136(C), pages 856-864.
    • Handle: RePEc:eee:renene:v:136:y:2019:i:c:p:856-864
    DOI: 10.1016/j.renene.2019.01.052
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    1. Amani, H. & Ahmad, Z. & Hameed, B.H., 2014. "Synthesis of fatty acid methyl esters via the methanolysis of palm oil over Ca3.5xZr0.5yAlxO3 mixed oxide catalyst," Renewable Energy, Elsevier, vol. 66(C), pages 680-685.
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    6. Yusuff, Adeyinka Sikiru & Gbadamosi, Afeez Olayinka & Atray, Neeraj, 2022. "Development of a zeolite supported CaO derived from chicken eggshell as active base catalyst for used cooking oil biodiesel production," Renewable Energy, Elsevier, vol. 197(C), pages 1151-1162.
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