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Waste quail beaks as renewable source for synthesizing novel catalysts for biodiesel production

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  • Khan, Haris Mahmood
  • Iqbal, Tanveer
  • Ali, Chaudhry Haider
  • Yasin, Saima
  • Jamil, Farrukh

Abstract

In the current study, waste biomass (quail beaks) has been considered for synthesizing highly active hydroxyapatite (HAp) catalyst and used for biodiesel production. The produced HAp is characterized by several analytical techniques such as Thermogravimetric analysis/differential scanning calorimetry (TGA/DSC), X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), Scanning electron microscopy (SEM), Energy dispersive X-ray spectroscopy (EDX), Hammett indicator-benzene benzoic acid titration method and BET surface area. TGA/DSC analysis confirmed the complete removal of organic matter from the raw quail beaks. The XRD results revealed that the crystallinity of HAp phase was enhanced by thermal calcination with crystallite size of 37.33 nm at 900 °C. FTIR results showed the peaks of phosphate (PO4−3) and hydroxyl groups (OH−1) belonging to HAp molecules. EDX analysis revealed the presence of calcium (Ca) and phosphorus (P) compositions were 28.5 and 11.4 wt %, respectively. Total basicity and BET surface area of the synthesized catalyst were found to be 12.9 mmol/g and 4.54 m2/g, respectively. Furthermore, the treated HAp at temperature of 900 °C was used for biodiesel production from canola oil, rapeseed oil and waste cooking oil. Thus, HAp was opted to be highly active for biodiesel production with promising reusability.

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  • Khan, Haris Mahmood & Iqbal, Tanveer & Ali, Chaudhry Haider & Yasin, Saima & Jamil, Farrukh, 2020. "Waste quail beaks as renewable source for synthesizing novel catalysts for biodiesel production," Renewable Energy, Elsevier, vol. 154(C), pages 1035-1043.
    • Handle: RePEc:eee:renene:v:154:y:2020:i:c:p:1035-1043
    DOI: 10.1016/j.renene.2020.03.079
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    References listed on IDEAS

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    1. Tan, Yie Hua & Abdullah, Mohammad Omar & Nolasco-Hipolito, Cirilo & Taufiq-Yap, Yun Hin, 2015. "Waste ostrich- and chicken-eggshells as heterogeneous base catalyst for biodiesel production from used cooking oil: Catalyst characterization and biodiesel yield performance," Applied Energy, Elsevier, vol. 160(C), pages 58-70.
    2. Farooq, Muhammad & Ramli, Anita & Naeem, Abdul, 2015. "Biodiesel production from low FFA waste cooking oil using heterogeneous catalyst derived from chicken bones," Renewable Energy, Elsevier, vol. 76(C), pages 362-368.
    3. kumar, Mukesh & Sharma, Mahendra Pal, 2016. "Selection of potential oils for biodiesel production," Renewable and Sustainable Energy Reviews, Elsevier, vol. 56(C), pages 1129-1138.
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