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Biodiesel production in a novel continuous flow microwave reactor

Author

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  • Choedkiatsakul, I.
  • Ngaosuwan, K.
  • Assabumrungrat, S.
  • Mantegna, S.
  • Cravotto, G.

Abstract

This paper presents the use of a commercial FlowSynth microwave reactor for the continuous production of biodiesel from palm oil. A high ester content of 99.4% can be obtained in only 1.75 min residence time at a methanol to oil molar ratio of 12, a microwave heating power of 400 W, reaction temperature of 70 °C and NaOH catalyst loading of 1%wt of oil. The process energy consumption has also been investigated in order to assess the potential advantages of using microwave irradiation for biodiesel production. The energy consumption of palm oil transesterification as low as 0.1167 kWh/L of biodiesel was required, proving that microwave reactors need less energy consumption as compared to conventional processes. Moreover, all main biodiesel properties are in accordance with EN/ASTM standards.

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  • Choedkiatsakul, I. & Ngaosuwan, K. & Assabumrungrat, S. & Mantegna, S. & Cravotto, G., 2015. "Biodiesel production in a novel continuous flow microwave reactor," Renewable Energy, Elsevier, vol. 83(C), pages 25-29.
    • Handle: RePEc:eee:renene:v:83:y:2015:i:c:p:25-29
    DOI: 10.1016/j.renene.2015.04.012
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    References listed on IDEAS

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    1. Motasemi, F. & Ani, F.N., 2012. "A review on microwave-assisted production of biodiesel," Renewable and Sustainable Energy Reviews, Elsevier, vol. 16(7), pages 4719-4733.
    2. Liu, Junhai & Zhuang, Yingbin & Li, Yan & Chen, Limei & Guo, Jingxue & Li, Demao & Ye, Naihao, 2013. "Optimizing the conditions for the microwave-assisted direct liquefaction of Ulva prolifera for bio-oil production using response surface methodology," Energy, Elsevier, vol. 60(C), pages 69-76.
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    1. Saba, Tony & Estephane, Jane & El Khoury, Bilal & El Khoury, Maroulla & Khazma, Mahmoud & El Zakhem, Henri & Aouad, Samer, 2016. "Biodiesel production from refined sunflower vegetable oil over KOH/ZSM5 catalysts," Renewable Energy, Elsevier, vol. 90(C), pages 301-306.
    2. Aghel, Babak & Mohadesi, Majid & Ansari, Ahmadreza & Maleki, Mahmoud, 2019. "Pilot-scale production of biodiesel from waste cooking oil using kettle limescale as a heterogeneous catalyst," Renewable Energy, Elsevier, vol. 142(C), pages 207-214.
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    4. Ahmad Abbaszadeh-Mayvan & Barat Ghobadian & Gholamhassan Najafi & Talal Yusaf, 2018. "Intensification of Continuous Biodiesel Production from Waste Cooking Oils Using Shockwave Power Reactor: Process Evaluation and Optimization through Response Surface Methodology (RSM)," Energies, MDPI, vol. 11(10), pages 1-13, October.
    5. Silitonga, A.S. & Shamsuddin, A.H. & Mahlia, T.M.I. & Milano, Jassinne & Kusumo, F. & Siswantoro, Joko & Dharma, S. & Sebayang, A.H. & Masjuki, H.H. & Ong, Hwai Chyuan, 2020. "Biodiesel synthesis from Ceiba pentandra oil by microwave irradiation-assisted transesterification: ELM modeling and optimization," Renewable Energy, Elsevier, vol. 146(C), pages 1278-1291.
    6. Phromphithak, Sanphawat & Meepowpan, Puttinan & Shimpalee, Sirivatch & Tippayawong, Nakorn, 2020. "Transesterification of palm oil into biodiesel using ChOH ionic liquid in a microwave heated continuous flow reactor," Renewable Energy, Elsevier, vol. 154(C), pages 925-936.
    7. Nayak, Sheetal N. & Bhasin, Chandra Prakash & Nayak, Milap G., 2019. "A review on microwave-assisted transesterification processes using various catalytic and non-catalytic systems," Renewable Energy, Elsevier, vol. 143(C), pages 1366-1387.
    8. Idowu, Ibijoke & Pedrola, Montserrat Ortoneda & Wylie, Steve & Teng, K.H. & Kot, Patryk & Phipps, David & Shaw, Andy, 2019. "Improving biodiesel yield of animal waste fats by combination of a pre-treatment technique and microwave technology," Renewable Energy, Elsevier, vol. 142(C), pages 535-542.
    9. R, Gopi & Thangarasu, Vinoth & Vinayakaselvi M, Angkayarkan & Ramanathan, Anand, 2022. "A critical review of recent advancements in continuous flow reactors and prominent integrated microreactors for biodiesel production," Renewable and Sustainable Energy Reviews, Elsevier, vol. 154(C).
    10. Soltani, Soroush & Roodbar Shojaei, Taha & Khanian, Nasrin & Shean Yaw Choong, Thomas & Asim, Nilofar & Zhao, Yue, 2022. "Artificial neural network method modeling of microwave-assisted esterification of PFAD over mesoporous TiO2‒ZnO catalyst," Renewable Energy, Elsevier, vol. 187(C), pages 760-773.
    11. Tran, Dang-Thuan & Chang, Jo-Shu & Lee, Duu-Jong, 2017. "Recent insights into continuous-flow biodiesel production via catalytic and non-catalytic transesterification processes," Applied Energy, Elsevier, vol. 185(P1), pages 376-409.
    12. Silitonga, A.S. & Mahlia, T.M.I. & Kusumo, F. & Dharma, S. & Sebayang, A.H. & Sembiring, R.W. & Shamsuddin, A.H., 2019. "Intensification of Reutealis trisperma biodiesel production using infrared radiation: Simulation, optimisation and validation," Renewable Energy, Elsevier, vol. 133(C), pages 520-527.

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