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Pilot-scale production of biodiesel from waste cooking oil using kettle limescale as a heterogeneous catalyst

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  • Aghel, Babak
  • Mohadesi, Majid
  • Ansari, Ahmadreza
  • Maleki, Mahmoud

Abstract

This study aimed to evaluate and optimize a pilot-scale microreactor to convert waste cooking oil (WCO) into biodiesel using kettle limescale. Box-Behnken design was used to determine the optimum conditions for producing biodiesel. Effects of main variables including reaction temperature, catalyst concentration, and alcohol/oil volume ratio were evaluated at a constant residence time of 10 min. Based on the results of analysis of variance, the quadratic regression model had the best coefficient of determination (R2=0.9930) and adjusted coefficient of determination (RAdj.2= 0.9804). After the optimization of temperature, catalyst concentration, and methanol/oil volume ratio, the residence time was optimized to achieve the maximum purity of the produced biodiesel. At a reaction temperature of 61.7 °C, catalysts concentration (oil based) of 8.87 wt %, methanol to oil volume ratio of 1.7:3, and a residence time of 15 min, we observed the optimal conditions for obtaining a maximum biodiesel purity of 93.41%.

Suggested Citation

  • Aghel, Babak & Mohadesi, Majid & Ansari, Ahmadreza & Maleki, Mahmoud, 2019. "Pilot-scale production of biodiesel from waste cooking oil using kettle limescale as a heterogeneous catalyst," Renewable Energy, Elsevier, vol. 142(C), pages 207-214.
    • Handle: RePEc:eee:renene:v:142:y:2019:i:c:p:207-214
    DOI: 10.1016/j.renene.2019.04.100
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    3. R, Gopi & Thangarasu, Vinoth & Vinayakaselvi M, Angkayarkan & Ramanathan, Anand, 2022. "A critical review of recent advancements in continuous flow reactors and prominent integrated microreactors for biodiesel production," Renewable and Sustainable Energy Reviews, Elsevier, vol. 154(C).
    4. Zheng, Yuanzhou & Shadloo, Mostafa Safdari & Nasiri, Hossein & Maleki, Akbar & Karimipour, Arash & Tlili, Iskander, 2020. "Prediction of viscosity of biodiesel blends using various artificial model and comparison with empirical correlations," Renewable Energy, Elsevier, vol. 153(C), pages 1296-1306.
    5. Siddharth Jain & Nitin Kumar & Varun Pratap Singh & Sachin Mishra & Naveen Kumar Sharma & Mohit Bajaj & T. M. Yunus Khan, 2023. "Transesterification of Algae Oil and Little Amount of Waste Cooking Oil Blend at Low Temperature in the Presence of NaOH," Energies, MDPI, vol. 16(3), pages 1-13, January.
    6. Ning, Yilin & Niu, Shengli & Wang, Yongzheng & Zhao, Jianli & Lu, Chunmei, 2021. "Sono-modified halloysite nanotube with NaAlO2 as novel heterogeneous catalyst for biodiesel production: Optimization via GA_BP neural network," Renewable Energy, Elsevier, vol. 175(C), pages 391-404.
    7. Mohadesi, Majid & Gouran, Ashkan & Dehghan Dehnavi, Amir, 2021. "Biodiesel production using low cost material as high effective catalyst in a microreactor," Energy, Elsevier, vol. 219(C).
    8. Zhang, Pingbo & Liu, Peng & Fan, Mingming & Jiang, Pingping & Haryono, Agus, 2021. "High-performance magnetite nanoparticles catalyst for biodiesel production: Immobilization of 12-tungstophosphoric acid on SBA-15 works effectively," Renewable Energy, Elsevier, vol. 175(C), pages 244-252.

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