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Kinetic study and thermal analysis of the pyrolysis of non-edible oilseed powders by thermogravimetric and differential scanning calorimetric analysis

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  • Shadangi, Krushna Prasad
  • Mohanty, Kaustubha

Abstract

This work reports the kinetic study of the pyrolysis of four non-edible oil seeds such as Mahua, Karanja, Niger and Linseed conducted at a heating rate of 5, 10 and 15 °C min−1 under nitrogen atmosphere. The relation between kinetic parameters and degradation rate was observed with respect to temperature and heating rate. The results indicated that the kinetic parameters were very close to each other and directly proportional to temperature and heating rate. The comparison of kinetic parameters related to heating rate concluded that heating rate had a direct affinity towards activation energy and pre-exponential factor. The TG-DTG analysis indicated three stages of thermal degradation during pyrolysis of the oil seeds whereas DSC analysis point towards the endothermic and exothermic pathway of pyrolysis. The presence of hemicelluloses, cellulose and lignin was determined on the basis of degradation temperature and their respective functional groups in the seeds observed by FTIR analysis.

Suggested Citation

  • Shadangi, Krushna Prasad & Mohanty, Kaustubha, 2014. "Kinetic study and thermal analysis of the pyrolysis of non-edible oilseed powders by thermogravimetric and differential scanning calorimetric analysis," Renewable Energy, Elsevier, vol. 63(C), pages 337-344.
    • Handle: RePEc:eee:renene:v:63:y:2014:i:c:p:337-344
    DOI: 10.1016/j.renene.2013.09.039
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    1. Van de Velden, Manon & Baeyens, Jan & Brems, Anke & Janssens, Bart & Dewil, Raf, 2010. "Fundamentals, kinetics and endothermicity of the biomass pyrolysis reaction," Renewable Energy, Elsevier, vol. 35(1), pages 232-242.
    2. Naik, Satyanarayan & Goud, Vaibhav V. & Rout, Prasant K. & Jacobson, Kathlene & Dalai, Ajay K., 2010. "Characterization of Canadian biomass for alternative renewable biofuel," Renewable Energy, Elsevier, vol. 35(8), pages 1624-1631.
    3. Chen, Wei-Hsin & Kuo, Po-Chih, 2011. "Isothermal torrefaction kinetics of hemicellulose, cellulose, lignin and xylan using thermogravimetric analysis," Energy, Elsevier, vol. 36(11), pages 6451-6460.
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