IDEAS home Printed from https://ideas.repec.org/a/eee/energy/v252y2022ics0360544222009653.html
   My bibliography  Save this article

Effect of final pyrolysis temperature on the composition and structure of shale oil: Synergistic use of multiple analysis and testing methods

Author

Listed:
  • Cui, Da
  • Yin, Helin
  • Liu, Yupeng
  • Li, Ji
  • Pan, Shuo
  • Wang, Qing

Abstract

As the focus of research on the pyrolysis mechanism of oil shale shifting towards the molecular level, identifying the effect of pyrolysis temperature on the molecular composition and structure becomes all the more important. In this study, the molecular characteristics of shale oils produced at different final pyrolysis temperatures was compared and analyzed through synergistic use of multiple analysis and testing methods. The results showed that compared with the traditional gas chromatography-mass spectrometry (GC-MS), comprehensive two-dimensional gas chromatography-time of flight mass spectrometry (GC × GC-TOF/MS) has obvious advantages in the characterization of heteroatoms and cycloalkanes. Fourier transform infrared spectrometry (FT-IR) can supplement the deficiency of nuclear magnetic resonance (NMR) in the characterization of oxygen-containing functional groups. With the increase in final temperature, the aromatization reaction of cycloalkanes intensified. Conversely, the degree of alkane branching and carbon chain length decreased. Based upon mutual verification and supplement of various analysis results, a novel method was proposed for the comprehensive molecular characterization of complex liquid fuel oil. According to the advantages and characteristics of different detection methods, synergistic use of multiple methods for different fractions is an important research direction for the molecular characterization of complex liquid fuel oil in the future.

Suggested Citation

  • Cui, Da & Yin, Helin & Liu, Yupeng & Li, Ji & Pan, Shuo & Wang, Qing, 2022. "Effect of final pyrolysis temperature on the composition and structure of shale oil: Synergistic use of multiple analysis and testing methods," Energy, Elsevier, vol. 252(C).
    • Handle: RePEc:eee:energy:v:252:y:2022:i:c:s0360544222009653
    DOI: 10.1016/j.energy.2022.124062
    as

    Download full text from publisher

    File URL: http://www.sciencedirect.com/science/article/pii/S0360544222009653
    Download Restriction: Full text for ScienceDirect subscribers only
    File URL: https://libkey.io/10.1016/j.energy.2022.124062?utm_source=ideas
    LibKey link: if access is restricted and if your library uses this service, LibKey will redirect you to where you can use your library subscription to access this item
    ---><---

    As the access to this document is restricted, you may want to search for a different version of it.

    References listed on IDEAS

    as
    1. Aghel, Babak & Gouran, Ashkan & Nasirmanesh, Farzad, 2022. "Transesterification of waste cooking oil using clinoptilolite/ industrial phosphoric waste as green and environmental catalysts," Energy, Elsevier, vol. 244(PB).
    2. Luo, Wei & Hu, Qing & Fan, Zhong-yi & Wan, Jun & He, Qian & Huang, Sheng-xiong & Zhou, Nan & Song, Min & Zhang, Jia-chao & Zhou, Zhi, 2020. "The effect of different particle sizes and HCl-modified kaolin on catalytic pyrolysis characteristics of reworked polypropylene plastics," Energy, Elsevier, vol. 213(C).
    3. Kang, Shijie & Sun, Youhong & Qiao, Mingyang & Li, Shengli & Deng, Sunhua & Guo, Wei & Li, Jiasheng & He, Wentong, 2022. "The enhancement on oil shale extraction of FeCl3 catalyst in subcritical water," Energy, Elsevier, vol. 238(PA).
    4. Merckel, Ryan D. & Heydenrych, Mike D. & Sithole, Bruce B., 2021. "Pyrolysis oil composition and catalytic activity estimated by cumulative mass analysis using Py-GC/MS EGA-MS," Energy, Elsevier, vol. 219(C).
    5. Tariq, Muhammad & Qureshi, Ahmad Kaleem & Karim, Shaista & Sirajuddin, Muhammad & Abbas, Naseem & Imran, Muhammad & Shirazi, Jaffir Hussain, 2021. "Synthesis, characterization and fuel parameters analysis of linseed oil biodiesel using cadmium oxide nanoparticles," Energy, Elsevier, vol. 222(C).
    6. Hu, Liangdong & Ma, Longlong & Hu, Guangzhi & Zhang, Wenjie & Liu, Ying & Xu, Rui & Ge, Wen & Chen, Yubao, 2022. "Utilization of illumination and thermal field in the preparation of jet–fuel components: The photothermic catalysis of Jatropha oil over the M/TiO2–HZSM–5," Energy, Elsevier, vol. 239(PC).
    Full references (including those not matched with items on IDEAS)

    Citations

    Citations are extracted by the CitEc Project, subscribe to its RSS feed for this item.
    as


    Cited by:

    1. Wei, Jianguang & Yang, Erlong & Li, Jiangtao & Liang, Shuang & Zhou, Xiaofeng, 2023. "Nuclear magnetic resonance study on the evolution of oil water distribution in multistage pore networks of shale oil reservoirs," Energy, Elsevier, vol. 282(C).
    2. de Brito, Vitor Lima & Gonçalves, Matheus Arrais & dos Santos, Hiarla Cristina Lima & da Rocha Filho, Geraldo Narciso & da Conceição, Leyvison Rafael Vieira, 2023. "Biodiesel production from waste frying oil using molybdenum over niobia as heterogeneous acid catalyst: Process optimization and kinetics study," Renewable Energy, Elsevier, vol. 215(C).
    3. Chang, Lei & Mohsin, Muhammad & Gao, Zhennan & Taghizadeh-Hesary, Farhad, 2023. "Asymmetric impact of oil price on current account balance: Evidence from oil importing countries," Energy Economics, Elsevier, vol. 123(C).
    4. Zhang, Le & Khishe, Mohammad & Mohammadi, Mokhtar & Mohammed, Adil Hussein, 2022. "Environmental economic dispatch optimization using niching penalized chimp algorithm," Energy, Elsevier, vol. 261(PA).
    5. Kang, Shijie & Zhang, Shijing & Wang, Zhendong & Li, Shengli & Zhao, Fangci & Yang, Jie & Zhou, Lingbo & Deng, Yang & Sun, Guidong & Yu, Hongdong, 2023. "Highly efficient catalytic pyrolysis of oil shale by CaCl2 in subcritical water," Energy, Elsevier, vol. 274(C).
    6. Wei, Jianguang & Zhang, Dong & Zhang, Xin & Zhao, Xiaoqing & Zhou, Runnan, 2023. "Experimental study on water flooding mechanism in low permeability oil reservoirs based on nuclear magnetic resonance technology," Energy, Elsevier, vol. 278(PB).

    Most related items

    These are the items that most often cite the same works as this one and are cited by the same works as this one.
    1. Nahas, Lea & Dahdah, Eliane & Aouad, Samer & El Khoury, Bilal & Gennequin, Cedric & Abi Aad, Edmond & Estephane, Jane, 2023. "Highly efficient scallop seashell-derived catalyst for biodiesel production from sunflower and waste cooking oils: Reaction kinetics and effect of calcination temperature studies," Renewable Energy, Elsevier, vol. 202(C), pages 1086-1095.
    2. Wang, Lei & Yang, Dong & Zhang, Yuxing & Li, Wenqing & Kang, Zhiqin & Zhao, Yangsheng, 2022. "Research on the reaction mechanism and modification distance of oil shale during high-temperature water vapor pyrolysis," Energy, Elsevier, vol. 261(PB).
    3. Saikia, Kankana & Das, Arpita & Sema, Atoholi H. & Basumatary, Sanjay & Shaemningwar Moyon, N. & Mathimani, Thangavel & Rokhum, Samuel Lalthazuala, 2024. "Response surface optimization, kinetics, thermodynamics, and life cycle cost analysis of biodiesel production from Jatropha curcas oil using biomass-based functional activated carbon catalyst," Renewable Energy, Elsevier, vol. 229(C).
    4. Wang, Zhijuan & Zhou, Huajing & Liu, Zilian & Miao, Rongrong & He, Liang & Guan, Qingqing, 2023. "Walnut-shaped calcium oxide-cancrinite spheres for transesterification of waste frying oil," Renewable Energy, Elsevier, vol. 208(C), pages 229-239.
    5. Cui, Yunlei & Zhang, Yaning & Cui, Longfei & Xiong, Qingang & Mostafa, Ehab, 2023. "Microwave-assisted fluidized bed reactor pyrolysis of polypropylene plastic for pyrolysis gas production towards a sustainable development," Applied Energy, Elsevier, vol. 342(C).
    6. Ricardo de C. Bittencourt & Tiago Guimarães & Marcelo M. da Costa & Larissa S. Silva & Verônica O. de P. Barbosa & Stéphani Caroline de L. Arêdes & Krisnna S. Alves & Ana Márcia M. L. Carvalho, 2024. "Production of High-Value Green Chemicals via Catalytic Fast Pyrolysis of Eucalyptus urograndis Forest Residues," Sustainability, MDPI, vol. 16(19), pages 1-14, September.
    7. Zhang, Xu & Guo, Wei & Pan, Junfan & Zhu, Chaofan & Deng, Sunhua, 2024. "In-situ pyrolysis of oil shale in pressured semi-closed system: Insights into products characteristics and pyrolysis mechanism," Energy, Elsevier, vol. 286(C).
    8. Torkzaban, Sama & Feyzi, Mostafa & norouzi, Leila, 2022. "A novel robust CaO/ZnFe2O4 hollow magnetic microspheres heterogenous catalyst for synthesis biodiesel from waste frying sunflower oil," Renewable Energy, Elsevier, vol. 200(C), pages 996-1007.
    9. Ming-Chien Hsiao & Peir-Horng Liao & Kuo-Chou Yang & Nguyen Vu Lan & Shuhn-Shyurng Hou, 2022. "Enhanced Biodiesel Synthesis via a Homogenizer-Assisted Two-Stage Conversion Process Using Waste Edible Oil as Feedstock," Energies, MDPI, vol. 15(23), pages 1-15, November.
    10. Kang, Shijie & Zhang, Shijing & Wang, Zhendong & Li, Shengli & Zhao, Fangci & Yang, Jie & Zhou, Lingbo & Deng, Yang & Sun, Guidong & Yu, Hongdong, 2023. "Highly efficient catalytic pyrolysis of oil shale by CaCl2 in subcritical water," Energy, Elsevier, vol. 274(C).
    11. Aghel, Babak & Biabani, Arash, 2024. "Using solar microreactors and photocatalysts to synthesize biodiesel," Renewable Energy, Elsevier, vol. 220(C).
    12. Hu, Zhiyuan & Wang, Zizhou & Luo, Jun & Fu, Jiale & Tan, Piqiang & Lou, Diming, 2023. "Effect of transport distance on the size distribution, graphitized structure, surface functional groups and oxidation activity of PM from diesel engine: A comparison of waste cooking oil biodiesel and," Energy, Elsevier, vol. 282(C).
    13. Rongsheng Zhao & Luquan Ren & Sunhua Deng & Youhong Sun & Zhiyong Chang, 2021. "Constrain on Oil Recovery Stage during Oil Shale Subcritical Water Extraction Process Based on Carbon Isotope Fractionation Character," Energies, MDPI, vol. 14(23), pages 1-12, November.
    14. Ruatpuia, Joseph V.L. & Changmai, Bishwajit & Pathak, Ayush & Alghamdi, Lana A. & Kress, Thomas & Halder, Gopinath & Wheatley, Andrew E.H. & Rokhum, Samuel Lalthazuala, 2023. "Green biodiesel production from Jatropha curcas oil using a carbon-based solid acid catalyst: A process optimization study," Renewable Energy, Elsevier, vol. 206(C), pages 597-608.
    15. Hong, Dikun & Li, Ping & Si, Ting & Guo, Xin, 2021. "ReaxFF simulations of the synergistic effect mechanisms during co-pyrolysis of coal and polyethylene/polystyrene," Energy, Elsevier, vol. 218(C).
    16. Tang, Hongbiao & Lin, Jiayu & Cao, Yang & Jibran, Khalil & Li, Jin, 2022. "Influence of NiMoP phase on hydrodeoxygenation pathways of jatropha oil," Energy, Elsevier, vol. 243(C).
    17. Xing, Shiyou & Fu, Junying & Li, Ming & Yang, Gaixiu & Lv, Pengmei, 2024. "Emerging catalysis in solvent-free hydrodeoxygenation of waste lipids under mild conditions: A review," Renewable and Sustainable Energy Reviews, Elsevier, vol. 200(C).
    18. Luo, Wei & Dong, Hang & Wang, Tao & Zhang, Siyan & Zhang, Dongyu & Li, Bo & Huang, Sheng & Hu, Jian & Song, Min & Zhou, Zhi, 2022. "Co-pyrolysis of Chinese herb residue and polypropylene over Ni, Fe, Co and Cu/AC: Co-production and formation mechanism of carbon nanomaterials, liquid oil and pyrolysis gas," Energy, Elsevier, vol. 244(PA).
    19. Perumal, Govindhan, 2024. "Production of biodiesel from waste cooking oil using a novel surface-functionalized CaMoO4/ TiO2 solid catalyst," Renewable Energy, Elsevier, vol. 228(C).
    20. Muzyka, Roksana & Misztal, Edyta & Hrabak, Joanna & Banks, Scott W. & Sajdak, Marcin, 2023. "Various biomass pyrolysis conditions influence the porosity and pore size distribution of biochar," Energy, Elsevier, vol. 263(PE).

    Corrections

    All material on this site has been provided by the respective publishers and authors. You can help correct errors and omissions. When requesting a correction, please mention this item's handle: RePEc:eee:energy:v:252:y:2022:i:c:s0360544222009653. See general information about how to correct material in RePEc.

    If you have authored this item and are not yet registered with RePEc, we encourage you to do it here. This allows to link your profile to this item. It also allows you to accept potential citations to this item that we are uncertain about.

    If CitEc recognized a bibliographic reference but did not link an item in RePEc to it, you can help with this form .

    If you know of missing items citing this one, you can help us creating those links by adding the relevant references in the same way as above, for each refering item. If you are a registered author of this item, you may also want to check the "citations" tab in your RePEc Author Service profile, as there may be some citations waiting for confirmation.

    For technical questions regarding this item, or to correct its authors, title, abstract, bibliographic or download information, contact: Catherine Liu (email available below). General contact details of provider: http://www.journals.elsevier.com/energy .

    Please note that corrections may take a couple of weeks to filter through the various RePEc services.

    IDEAS is a RePEc service. RePEc uses bibliographic data supplied by the respective publishers.