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Preparation and performance of amine-based polyacrylamide composite beads for CO2 capture

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  • Nie, Lijuan
  • Jin, Junsu
  • Chen, Jian
  • Mi, Jianguo

Abstract

The macropore composite beads were prepared as CO2 adsorbent by polymerization of polyacrylamide and impregnation of 1,2-epoxyhexane functionalized poly(ethyleneimine). The consecutive CO2 adsorption-desorption tests were performed at 1 bar in the range of 50–125 °C. The time required to achieve 90% CO2 uptake (2.64 mmol·g−1) is less than 10 min, and 90% CO2 desorption can be realized within 11 min. After 50 cycles of adsorption-desorption, the adsorption capacity declines 9.2 wt.%. According to the adsorption-desorption thermodynamics without consideration of the heat recovery, the calculated regeneration heat is 2.2 MJ·kg−1(CO2). The attrition resistance of the spherical beads was tested in a bubbling fluidized-bed reactor, and the attrition ratio is 0.30 wt.%·h−1 at 130 °C. These results indicate that the synthesized adsorbent possesses high adsorption efficiency, low desorption energy, and good attrition resistance performance, showing good application prospects for CO2 capture in fluidized-bed reactors.

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  • Nie, Lijuan & Jin, Junsu & Chen, Jian & Mi, Jianguo, 2018. "Preparation and performance of amine-based polyacrylamide composite beads for CO2 capture," Energy, Elsevier, vol. 161(C), pages 60-69.
    • Handle: RePEc:eee:energy:v:161:y:2018:i:c:p:60-69
    DOI: 10.1016/j.energy.2018.07.116
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    References listed on IDEAS

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    Cited by:

    1. Xu, Chenhuan & Zhang, Yongmin & Yang, Tianlei & Jia, Xiaohao & Qiu, Feng & Liu, Cenfan & Jiang, Shuai, 2023. "Adsorption mechanisms and regeneration heat analysis of a solid amine sorbent during CO2 capture in wet flue gas," Energy, Elsevier, vol. 284(C).
    2. Mukhtar, Ahmad & Ullah, Sami & Inayat, Abrar & Saqib, Sidra & Mellon, Nurhayati Binti & Assiri, Mohammed Ali & Al-Sehemi, Abdullah G. & Khan Niazi, Muhammad Bilal & Jahan, Zaib & Bustam, Mohamad Azmi , 2021. "Synthesis-structure-property relationship of nitrogen-doped porous covalent triazine frameworks for pre-combustion CO2 capture," Energy, Elsevier, vol. 216(C).
    3. An, Xuefei & Li, Tongxin & Chen, Jiaqi & Fu, Dong, 2023. "3D-hierarchical porous functionalized carbon aerogel from renewable cellulose: An innovative solid-amine adsorbent with high CO2 adsorption performance," Energy, Elsevier, vol. 274(C).

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