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Preparation and performance of amine-based polyacrylamide composite beads for CO2 capture

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  • Nie, Lijuan
  • Jin, Junsu
  • Chen, Jian
  • Mi, Jianguo

Abstract

The macropore composite beads were prepared as CO2 adsorbent by polymerization of polyacrylamide and impregnation of 1,2-epoxyhexane functionalized poly(ethyleneimine). The consecutive CO2 adsorption-desorption tests were performed at 1 bar in the range of 50–125 °C. The time required to achieve 90% CO2 uptake (2.64 mmol·g−1) is less than 10 min, and 90% CO2 desorption can be realized within 11 min. After 50 cycles of adsorption-desorption, the adsorption capacity declines 9.2 wt.%. According to the adsorption-desorption thermodynamics without consideration of the heat recovery, the calculated regeneration heat is 2.2 MJ·kg−1(CO2). The attrition resistance of the spherical beads was tested in a bubbling fluidized-bed reactor, and the attrition ratio is 0.30 wt.%·h−1 at 130 °C. These results indicate that the synthesized adsorbent possesses high adsorption efficiency, low desorption energy, and good attrition resistance performance, showing good application prospects for CO2 capture in fluidized-bed reactors.

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  • Nie, Lijuan & Jin, Junsu & Chen, Jian & Mi, Jianguo, 2018. "Preparation and performance of amine-based polyacrylamide composite beads for CO2 capture," Energy, Elsevier, vol. 161(C), pages 60-69.
    • Handle: RePEc:eee:energy:v:161:y:2018:i:c:p:60-69
    DOI: 10.1016/j.energy.2018.07.116
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    References listed on IDEAS

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    1. Mondal, Monoj Kumar & Balsora, Hemant Kumar & Varshney, Prachi, 2012. "Progress and trends in CO2 capture/separation technologies: A review," Energy, Elsevier, vol. 46(1), pages 431-441.
    2. Jung, Wonho & Park, Junhyung & Won, Wangyun & Lee, Kwang Soon, 2018. "Simulated moving bed adsorption process based on a polyethylenimine-silica sorbent for CO2 capture with sensible heat recovery," Energy, Elsevier, vol. 150(C), pages 950-964.
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    4. Zhang, Wenbin & Liu, Hao & Sun, Yuan & Cakstins, Janis & Sun, Chenggong & Snape, Colin E., 2016. "Parametric study on the regeneration heat requirement of an amine-based solid adsorbent process for post-combustion carbon capture," Applied Energy, Elsevier, vol. 168(C), pages 394-405.
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