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Using 13X, LiX, and LiPdAgX zeolites for CO2 capture from post-combustion flue gas

Author

Listed:
  • Chen, S.J.
  • Zhu, M.
  • Fu, Y.
  • Huang, Y.X.
  • Tao, Z.C.
  • Li, W.L.

Abstract

This work investigates the application of X zeolites for capturing CO2 from post-combustion flue gas. LiX and LiPdAgX zeolites were prepared by an ion-exchange method using 13X zeolite. X-ray diffraction analysis showed that all samples exhibited characteristic peaks of X zeolites, where the peak intensities increased in the order: LiPdAgX>LiX>13X. The enhanced intensity of the diffraction peaks can increase the activity of the X zeolites and improve their adsorption performance. Scanning electron microscopy imaging showed that the intergranular pore canals of LiPdAgX zeolite were more concentrated. Pore structure analysis indicated that addition of Li+ to the 13X zeolite enhanced the specific surface areas and pore volumes of the zeolites. Among the 13X, LiX, and LiPdAgX zeolites, LiPdAgX showed the highest CO2/N2selectivity, where the difference in the CO2 adsorption capacity was due to differences in the number of adsorption sites and thermal conductivities of the X zeolites. The CO2 breakthrough time increased in succession for the 13X, LiX, and LiPdAgX zeolites. The CO2/N2 separation factor of the LiPdAgX zeolite was twice that of the 13X zeolite at a CO2 concentration of 20vol.%. The temperature variations during the adsorption process were used to determine the regeneration energy and adsorption capacity of the X zeolites. LiPdAgX zeolite required less energy for regeneration than 13X zeolite and MEA. After regeneration, the separation factor of LiPdAgX zeolite remained at 6.38 for 20vol.% CO2 in the flue gas. Therefore, LiPdAgX zeolite can effectively capture CO2 from post-combustion flue gas to curtail the release of CO2 into the atmosphere.

Suggested Citation

  • Chen, S.J. & Zhu, M. & Fu, Y. & Huang, Y.X. & Tao, Z.C. & Li, W.L., 2017. "Using 13X, LiX, and LiPdAgX zeolites for CO2 capture from post-combustion flue gas," Applied Energy, Elsevier, vol. 191(C), pages 87-98.
    • Handle: RePEc:eee:appene:v:191:y:2017:i:c:p:87-98
    DOI: 10.1016/j.apenergy.2017.01.031
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