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Natural dolomite modified with carbon coating for cyclic high-temperature CO2 capture

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  • Wang, Ke
  • Hu, Xiumeng
  • Zhao, Pengfei
  • Yin, Zeguang

Abstract

An efficient MgO-stabilized CaO sorbent via the citric acid treated dolomite coupled with carbonization process (denoted as carbon coating) was developed for CO2 capture at high temperature. The citric acid was used as a carbon source to produce the coated carbon, which was expected to effectively prevent the crystallites (CaO and MgO) from sintering. The original dolomite and citric-acid-treated dolomite with subsequent calcination in air were also prepared for comparison. Different characterizations (thermal decomposition, phase composition, morphology, and nitrogen adsorption) were performed. The cyclic-CO2-capture performance was tested in a fix-bed reactor. During the carbonization in N2 atmosphere, the acidified dolomite transformed into carbon-coated, Mg-doped calcite, which could control thermal sintering and prevent the de-mixing of CaO and MgO in the secondary calcination step in air. Thus, the sorbent prepared using carbon coating achieved smaller grains, larger specific surface area and pore volume and more uniform distribution of CaO and MgO, which led to its superior activity and stability, compared to two reference sorbents.

Suggested Citation

  • Wang, Ke & Hu, Xiumeng & Zhao, Pengfei & Yin, Zeguang, 2016. "Natural dolomite modified with carbon coating for cyclic high-temperature CO2 capture," Applied Energy, Elsevier, vol. 165(C), pages 14-21.
    • Handle: RePEc:eee:appene:v:165:y:2016:i:c:p:14-21
    DOI: 10.1016/j.apenergy.2015.12.071
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    References listed on IDEAS

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    3. Shi, Jiewen & Li, Yingjie & Zhang, Qing & Ma, Xiaotong & Duan, Lunbo & Zhou, Xingang, 2017. "CO2 capture performance of a novel synthetic CaO/sepiolite sorbent at calcium looping conditions," Applied Energy, Elsevier, vol. 203(C), pages 412-421.
    4. Wang, Ke & Zhou, Zhongyun & Zhao, Pengfei & Yin, Zeguang & Su, Zhen & Sun, Ji, 2016. "Synthesis of a highly efficient Li4SiO4 ceramic modified with a gluconic acid-based carbon coating for high-temperature CO2 capture," Applied Energy, Elsevier, vol. 183(C), pages 1418-1427.
    5. Parvez, Ashak Mahmud & Hafner, Selina & Hornberger, Matthias & Schmid, Max & Scheffknecht, Günter, 2021. "Sorption enhanced gasification (SEG) of biomass for tailored syngas production with in-situ CO2 capture: Current status, process scale-up experiences and outlook," Renewable and Sustainable Energy Reviews, Elsevier, vol. 141(C).
    6. Wang, Ke & Zhou, Zhongyun & Zhao, Pengfei & Yin, Zeguang & Su, Zhen & Sun, Ji, 2017. "Molten sodium-fluoride-promoted high-performance Li4SiO4-based CO2 sorbents at low CO2 concentrations," Applied Energy, Elsevier, vol. 204(C), pages 403-412.
    7. Antzaras, Andy N. & Lemonidou, Angeliki A., 2022. "Recent advances on materials and processes for intensified production of blue hydrogen," Renewable and Sustainable Energy Reviews, Elsevier, vol. 155(C).
    8. Ortiz, C. & Chacartegui, R. & Valverde, J.M. & Becerra, J.A., 2016. "A new integration model of the calcium looping technology into coal fired power plants for CO2 capture," Applied Energy, Elsevier, vol. 169(C), pages 408-420.
    9. Ding, Jing & Yu, Chao & Lu, Jianfeng & Wei, Xiaolan & Wang, Weilong & Pan, Gechuanqi, 2020. "Enhanced CO2 adsorption of MgO with alkali metal nitrates and carbonates," Applied Energy, Elsevier, vol. 263(C).
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    11. Zhang, Wan & Li, Yingjie & He, Zirui & Ma, Xiaotong & Song, Haiping, 2017. "CO2 capture by carbide slag calcined under high-concentration steam and energy requirement in calcium looping conditions," Applied Energy, Elsevier, vol. 206(C), pages 869-878.

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    Keywords

    CO2 capture; Modification; Citric acid; Dolomite;
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