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One-pot assembly of sulfated lignin/Zr coordination polymer for efficient alcoholysis of furfuryl alcohol to methyl levulinate

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  • Xu, Yingying
  • Guo, Haixin
  • Qi, Xinhua

Abstract

Biomass-derived alkyl levulinates are considered to be ideal fuel additives, and the construction of green and economic catalysts for the production of alkyl levulinates was still a challenging goal. In this work, a facile method for the synthesis of sulfated lignin/Zr coordination polymer (Zr-LSNa@SX) was developed through the coordination of sodium lignosulfonate with Zr ions by hydrothermal procedure. The catalytic performance of prepared Zr-LSNa@SX for the direct conversion of furfuryl alcohol (FA) to methyl levulinate (ML) was studied and a 73.1 % yield of ML was achieved at 180 °C in 180 min. The as-prepared sulfated lignin/Zr coordination polymer was characterized using SEM, FT-IR, and Py-FTIR techniques, and it was determined that the Brønsted acid sites of the catalyst played a crucial role in the conversion of FA to ML in methanol. This work provided a facile method for constructing the green and economical bio-based solid acid catalyst which will greatly extend the application of bio-based materials in the acid-catalyzed reaction.

Suggested Citation

  • Xu, Yingying & Guo, Haixin & Qi, Xinhua, 2024. "One-pot assembly of sulfated lignin/Zr coordination polymer for efficient alcoholysis of furfuryl alcohol to methyl levulinate," Renewable Energy, Elsevier, vol. 229(C).
    • Handle: RePEc:eee:renene:v:229:y:2024:i:c:s0960148124008103
    DOI: 10.1016/j.renene.2024.120742
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    References listed on IDEAS

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    3. Tang, Yiwei & Liu, Xiaoning & Xi, Ran & Liu, Le & Qi, Xinhua, 2022. "Catalytic one-pot conversion of biomass-derived furfural to ethyl levulinate over bifunctional Nb/Ni@OMC," Renewable Energy, Elsevier, vol. 200(C), pages 821-831.
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