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Production of biodiesel from waste cooking oil using a homogeneous catalyst: Study of semi-industrial pilot of microreactor

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  • Mohadesi, Majid
  • Aghel, Babak
  • Maleki, Mahmoud
  • Ansari, Ahmadreza

Abstract

This study investigated the transesterification of waste cooking oil (WCO) with methanol in the presence of potassium hydroxide as the catalyst. A semi-industrial pilot of microreactor with 50 tubes with a diameter of 0.8 mm was used to produce 5 L/h biodiesel. Initially, the acidity of waste cooking oil was reduced to less than 1 mg KOH/g oil by using methanol at 60 °C in the presence of 1% sulfuric acid. Using Box-Behnken design method, the effects of methanol to oil molar ratio (6:1–12:1), catalyst weight (0.5–1.5 wt %), and reaction temperature (55–65 °C) were studied. The methanol to oil molar ratio of 9.4:1, the catalyst concentration of 1.16 wt %, and the reaction temperature of 62.4 °C was achieved under optimum condition. Finally, the effect of reaction time (30–120 s) was examined at the optimum condition. The highest level of biodiesel purity or fatty acid methyl esters % (FAMEs %) was 98.26%. In addition, the properties of produced biodiesel were determined and compared with those of the standard ASTM D6751.

Suggested Citation

  • Mohadesi, Majid & Aghel, Babak & Maleki, Mahmoud & Ansari, Ahmadreza, 2019. "Production of biodiesel from waste cooking oil using a homogeneous catalyst: Study of semi-industrial pilot of microreactor," Renewable Energy, Elsevier, vol. 136(C), pages 677-682.
    • Handle: RePEc:eee:renene:v:136:y:2019:i:c:p:677-682
    DOI: 10.1016/j.renene.2019.01.039
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    5. Mostafaei, Mostafa & Javadikia, Hossein & Naderloo, Leila, 2016. "Modeling the effects of ultrasound power and reactor dimension on the biodiesel production yield: Comparison of prediction abilities between response surface methodology (RSM) and adaptive neuro-fuzzy," Energy, Elsevier, vol. 115(P1), pages 626-636.
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    10. Siddharth Jain & Nitin Kumar & Varun Pratap Singh & Sachin Mishra & Naveen Kumar Sharma & Mohit Bajaj & T. M. Yunus Khan, 2023. "Transesterification of Algae Oil and Little Amount of Waste Cooking Oil Blend at Low Temperature in the Presence of NaOH," Energies, MDPI, vol. 16(3), pages 1-13, January.
    11. Monteiro, Rodolpho R.C. & Arana-Peña, Sara & da Rocha, Thays N. & Miranda, Letícia P. & Berenguer-Murcia, Ángel & Tardioli, Paulo W. & dos Santos, José C.S. & Fernandez-Lafuente, Roberto, 2021. "Liquid lipase preparations designed for industrial production of biodiesel. Is it really an optimal solution?," Renewable Energy, Elsevier, vol. 164(C), pages 1566-1587.
    12. Hájek, Martin & Vávra, Aleš & Skopal, František & Straková, Anna & Douda, Miroslav, 2020. "The description of catalyst behaviour during transesterification of rapeseed oil – Formation of micellar emulsion," Renewable Energy, Elsevier, vol. 159(C), pages 938-943.
    13. Phromphithak, Sanphawat & Meepowpan, Puttinan & Shimpalee, Sirivatch & Tippayawong, Nakorn, 2020. "Transesterification of palm oil into biodiesel using ChOH ionic liquid in a microwave heated continuous flow reactor," Renewable Energy, Elsevier, vol. 154(C), pages 925-936.
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