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Optimization of biodiesel production from camelina oil using orthogonal experiment

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  • Wu, Xuan
  • Leung, Dennis Y.C.

Abstract

Camelina oil is a low-cost feedstock for biodiesel production that has received a great deal of attention in recent years. This paper describes an optimization study on the production of biodiesel from camelina seed oil using alkaline transesterification. The optimization was based on sixteen well-planned orthogonal experiments (OA16 matrix). Four main process conditions in the transesterification reaction for obtaining the maximum biodiesel production yield (i.e. methanol quantity, reaction time, reaction temperature and catalyst concentration) were investigated. It was found that the order of significant factors for biodiesel production is catalyst concentration>reaction time>reaction temperature>methanol to oil ratio. Based on the results of the range analysis and analysis of variance (ANOVA), the maximum biodiesel yield was found at a molar ratio of methanol to oil of 8:1, a reaction time of 70min, a reaction temperature of 50°C, and a catalyst concentration of 1wt.%. The product and FAME yields of biodiesel under optimal conditions reached 95.8% and 98.4%, respectively. The properties of the optimized biodiesel, including density, kinematic viscosity, acid value, etc., were determined and compared with those produced from other oil feedstocks. The optimized biodiesel from camelina oil meets the relevant ASTM D6571 and EN 14214 biodiesel standards and can be used as a qualified fuel for diesel engines.

Suggested Citation

  • Wu, Xuan & Leung, Dennis Y.C., 2011. "Optimization of biodiesel production from camelina oil using orthogonal experiment," Applied Energy, Elsevier, vol. 88(11), pages 3615-3624.
    • Handle: RePEc:eee:appene:v:88:y:2011:i:11:p:3615-3624
    DOI: 10.1016/j.apenergy.2011.04.041
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    14. Iris Montero-Muñoz & David Mostaza-Colado & Aníbal Capuano & Pedro V. Mauri Ablanque, 2023. "Seed and Straw Characterization of Nine New Varieties of Camelina sativa (L.) Crantz," Land, MDPI, vol. 12(2), pages 1-12, January.
    15. Jahirul, M.I. & Rasul, M.G. & Brown, R.J. & Senadeera, W. & Hosen, M.A. & Haque, R. & Saha, S.C. & Mahlia, T.M.I., 2021. "Investigation of correlation between chemical composition and properties of biodiesel using principal component analysis (PCA) and artificial neural network (ANN)," Renewable Energy, Elsevier, vol. 168(C), pages 632-646.
    16. Marcela Bindzarova Gergelova & Zofia Kuzevicova & Slavomir Labant & Stefan Kuzevic & Diana Bobikova & Jozef Mizak, 2020. "Roof’s Potential and Suitability for PV Systems Based on LiDAR: A Case Study of Komárno, Slovakia," Sustainability, MDPI, vol. 12(23), pages 1-22, November.
    17. Lam, Man Kee & Lee, Keat Teong, 2012. "Potential of using organic fertilizer to cultivate Chlorella vulgaris for biodiesel production," Applied Energy, Elsevier, vol. 94(C), pages 303-308.
    18. Sendzikiene, Egle & Sinkuniene, Dovile & Kazanceva, Irina & Kazancev, Kiril, 2016. "Optimization of low quality rapeseed oil transesterification with butanol by applying the response surface methodology," Renewable Energy, Elsevier, vol. 87(P1), pages 266-272.
    19. Mathimani, Thangavel & Uma, Lakshmanan & Prabaharan, Dharmar, 2015. "Homogeneous acid catalysed transesterification of marine microalga Chlorella sp. BDUG 91771 lipid – An efficient biodiesel yield and its characterization," Renewable Energy, Elsevier, vol. 81(C), pages 523-533.
    20. Lian, Shuang & Li, Huijuan & Tang, Jinqiang & Tong, Dongmei & Hu, Changwei, 2012. "Integration of extraction and transesterification of lipid from jatropha seeds for the production of biodiesel," Applied Energy, Elsevier, vol. 98(C), pages 540-547.
    21. Lau, Pak-Chung & Kwong, Tsz-Lung & Yung, Ka-Fu, 2022. "Manganese glycerolate catalyzed simultaneous esterification and transesterification: The kinetic and mechanistic study, and application in biodiesel and bio-lubricants synthesis," Renewable Energy, Elsevier, vol. 189(C), pages 549-558.
    22. Xinhui Zhan & Liping Xiao & Bing Liang, 2019. "Experimental Study on the Optimum Preparation of Bentonite–Steel Slag Composite Particles," Sustainability, MDPI, vol. 12(1), pages 1-27, December.
    23. Long, Yun-Duo & Fang, Zhen & Su, Tong-Chao & Yang, Qing, 2014. "Co-production of biodiesel and hydrogen from rapeseed and Jatropha oils with sodium silicate and Ni catalysts," Applied Energy, Elsevier, vol. 113(C), pages 1819-1825.

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