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Synthesis of LiNi 0.85 Co 0.14 Al 0.01 O 2 Cathode Material and its Performance in an NCA/Graphite Full-Battery

Author

Listed:
  • Cornelius Satria Yudha

    (Department of Chemical Engineering, Faculty of Engineering, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta, Central Java 57126, Indonesia)

  • Soraya Ulfa Muzayanha

    (Department of Chemical Engineering, Faculty of Engineering, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta, Central Java 57126, Indonesia)

  • Hendri Widiyandari

    (Department of Physics, Faculty of Mathematic and Natural Science, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta, Central Java 57126, Indonesia
    National Center for Sustainable Transportation Technology, Institut Teknologi Bandung, Jl. Ganesha No.10, Bandung, West Java 40132, Indonesia)

  • Ferry Iskandar

    (National Center for Sustainable Transportation Technology, Institut Teknologi Bandung, Jl. Ganesha No.10, Bandung, West Java 40132, Indonesia
    Department of Physics, Institut Teknologi Bandung, Jl. Ganesha No.10, Bandung, West Java 40132, Indonesia)

  • Wahyudi Sutopo

    (National Center for Sustainable Transportation Technology, Institut Teknologi Bandung, Jl. Ganesha No.10, Bandung, West Java 40132, Indonesia
    Department of Industrial Engineering, Faculty of Engineering, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta, Central Java 57126, Indonesia)

  • Agus Purwanto

    (Department of Chemical Engineering, Faculty of Engineering, Universitas Sebelas Maret, Jl. Ir. Sutami 36 A, Surakarta, Central Java 57126, Indonesia
    National Center for Sustainable Transportation Technology, Institut Teknologi Bandung, Jl. Ganesha No.10, Bandung, West Java 40132, Indonesia)

Abstract

Nickel-rich cathode material, NCA (85:14:1), is successfully synthesized using two different, simple and economical batch methods, i.e., hydroxide co-precipitation (NCA-CP) and the hydroxides solid state reaction method (NCA-SS), followed by heat treatments. Based on the FTIR spectra, all precursor samples exhibit two functional groups of hydroxide and carbonate. The XRD patterns of NCA-CP and NCA-SS show a hexagonal layered structure (space group: R_3m), with no impurities detected. Based on the SEM images, the micro-sized particles exhibit a sphere-like shape with aggregates. The electrochemical performances of the samples were tested in a 18650-type full-cell battery using artificial graphite as the counter anode at the voltage range of 2.7–4.25 V. All samples have similar characteristics and electrochemical performances that are comparable to the commercial NCA battery, despite going through different synthesis routes. In conclusion, the overall results are considered good and have the potential to be adapted for commercialization.

Suggested Citation

  • Cornelius Satria Yudha & Soraya Ulfa Muzayanha & Hendri Widiyandari & Ferry Iskandar & Wahyudi Sutopo & Agus Purwanto, 2019. "Synthesis of LiNi 0.85 Co 0.14 Al 0.01 O 2 Cathode Material and its Performance in an NCA/Graphite Full-Battery," Energies, MDPI, vol. 12(10), pages 1-14, May.
    • Handle: RePEc:gam:jeners:v:12:y:2019:i:10:p:1886-:d:232101
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    References listed on IDEAS

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    3. Haipeng Li & Jiayi Wang & Yan Zhao & Taizhe Tan, 2018. "Synthesis of the ZnO@ZnS Nanorod for Lithium-Ion Batteries," Energies, MDPI, vol. 11(8), pages 1-8, August.
    4. Tao Cheng & Zhongtao Ma & Run Gu & Riming Chen & Yingchun Lyu & Anmin Nie & Bingkun Guo, 2018. "Cracks Formation in Lithium-Rich Cathode Materials for Lithium-Ion Batteries during the Electrochemical Process," Energies, MDPI, vol. 11(10), pages 1-10, October.
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    Cited by:

    1. Jun-Ping Hu & Hang Sheng & Qi Deng & Qiang Ma & Jun Liu & Xiong-Wei Wu & Jun-Jie Liu & Yu-Ping Wu, 2020. "High-Rate Layered Cathode of Lithium-Ion Batteries through Regulating Three-Dimensional Agglomerated Structure," Energies, MDPI, vol. 13(7), pages 1-12, April.

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