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The relationship between acidity, dispersion of nickel, and performance of Ni/Al-SBA-15 catalyst on eugenol hydrodeoxygenation

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  • Li, Xiangping
  • Chen, Lei
  • Chen, Guanyi
  • Zhang, Jianguang
  • Liu, Juping

Abstract

Catalytic hydrodeoxygenation (HDO) is considered as one of the most efficient methods for lignin-derived bio-oils upgrading. To reveal the relationship between the characters of Ni/Al-SBA-15 and the catalytic activity of eugenol hydrodeoxygenation in aqueous phase, Al-SBA-15 with different Si/Al ratios were synthesized using acid free method and corresponding Ni/Al-SBA-15 catalysts were prepared by incipient wetness impregnation method. The physicochemical characteristics were obtained by advanced instruments. The highest degree of nickel dispersion on Al-SBA-15 was obtained when the Si/Al ratio was 132 and the corresponding smallest average active nickel particle diameter is 38 nm. The adsorption and dispersion of nickel onto Al-SBA-15 was significantly relevant with the ratios of Brønsted acid site to Lewis acid site as well as the ratios of weak acid site to strong acid site. HDO experiments were carried out over Ni/Al-SBA-15 with different Si/Al ratios. 16Ni/S2-R catalyst with high quantity of acid sites and good dispersion of nickel showed high catalytic activity during hydrodeoxygenation of eugenol. A possible reaction mechanism was concluded based on the reaction results.

Suggested Citation

  • Li, Xiangping & Chen, Lei & Chen, Guanyi & Zhang, Jianguang & Liu, Juping, 2020. "The relationship between acidity, dispersion of nickel, and performance of Ni/Al-SBA-15 catalyst on eugenol hydrodeoxygenation," Renewable Energy, Elsevier, vol. 149(C), pages 609-616.
    • Handle: RePEc:eee:renene:v:149:y:2020:i:c:p:609-616
    DOI: 10.1016/j.renene.2019.12.094
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    1. Chen, Shuang & Miao, Caixia & Luo, Yan & Zhou, Guilin & Xiong, Kun & Jiao, Zhaojie & Zhang, Xianming, 2018. "Study of catalytic hydrodeoxygenation performance of Ni catalysts: Effects of prepared method," Renewable Energy, Elsevier, vol. 115(C), pages 1109-1117.
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    2. Tai, Lingyu & Hamidi, Roya & de Caprariis, Benedetta & Damizia, Martina & Paglia, Laura & Scarsella, Marco & Karimzadeh, Ramin & De Filippis, Paolo, 2022. "Guaiacol hydrotreating with in-situ generated hydrogen over ni/modified zeolite supports," Renewable Energy, Elsevier, vol. 182(C), pages 647-658.
    3. Gollakota, Anjani R.K. & Shu, Chi-Min & Sarangi, Prakash Kumar & Shadangi, Krushna Prasad & Rakshit, Sudip & Kennedy, John F. & Gupta, Vijai Kumar & Sharma, Minaxi, 2023. "Catalytic hydrodeoxygenation of bio-oil and model compounds - Choice of catalysts, and mechanisms," Renewable and Sustainable Energy Reviews, Elsevier, vol. 187(C).
    4. Chen, Guanyi & Liu, Juping & Li, Xiangping & Zhang, Jianguang & Yin, Han & Su, Zhenping, 2020. "Investigation on catalytic hydrodeoxygenation of eugenol blend with light fraction in bio-oil over Ni-based catalysts," Renewable Energy, Elsevier, vol. 157(C), pages 456-465.

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