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Volatile-char interactions during biomass pyrolysis: Effect of char preparation temperature

Author

Listed:
  • Li, Bin
  • Zhao, Lijun
  • Xie, Xing
  • Lin, Dan
  • Xu, Huibin
  • Wang, Shuang
  • Xu, Zhixiang
  • Wang, Junfeng
  • Huang, Yong
  • Zhang, Shu
  • Hu, Xun
  • Liu, Dongjing

Abstract

In this study, the effect of char preparation temperature on the interactions between cellulose volatiles and acid-washed sawdust char was investigated experimentally on a fixed-bed pyrolysis system. The results indicated that significant volatile-char interactions did exist at the pyrolysis temperature of 500 °C as evidenced by the great changes in the composition and distribution of pyrolysis products. The oxygen-containing functional groups as well as the aromatic ring systems in the char both acted as active sites during the volatile-char interactions. The changes in chemical structure of biochar caused by the different preparation temperatures would notably affect the final products of cellulose pyrolysis. Meanwhile, the acid-washed sawdust char was still found to participate in the reaction process, lower temperature chars would have higher reactivities, and an obvious weight loss of char was also observed after interactions. In addition, volatile-char interactions significantly increased the yields of non-condensable gases, especially those of CO and CO2, while decreased the yield of condensable vapors. The introduction of biochar into cellulose pyrolysis could promote the ring scission of pyranoses as well as the decarbonylation/decarboxylation and dehydration reactions, thus caused the yields of anhydrosugars and monoaromatic compounds decreased and the yields of light ketones and acids increased.

Suggested Citation

  • Li, Bin & Zhao, Lijun & Xie, Xing & Lin, Dan & Xu, Huibin & Wang, Shuang & Xu, Zhixiang & Wang, Junfeng & Huang, Yong & Zhang, Shu & Hu, Xun & Liu, Dongjing, 2021. "Volatile-char interactions during biomass pyrolysis: Effect of char preparation temperature," Energy, Elsevier, vol. 215(PB).
  • Handle: RePEc:eee:energy:v:215:y:2021:i:pb:s0360544220322969
    DOI: 10.1016/j.energy.2020.119189
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    References listed on IDEAS

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    1. Dhyani, Vaibhav & Bhaskar, Thallada, 2018. "A comprehensive review on the pyrolysis of lignocellulosic biomass," Renewable Energy, Elsevier, vol. 129(PB), pages 695-716.
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    3. Jiao, Zixin & Qiu, Penghua & Chen, Xiye & Liu, Li & Zhang, Linyao & Xing, Chang, 2023. "Effects of volatiles and active AAEMs interaction with char on char characteristics during co-pyrolysis," Renewable Energy, Elsevier, vol. 208(C), pages 618-626.
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    5. Magoua Mbeugang, Christian Fabrice & Li, Bin & Lin, Dan & Xie, Xing & Wang, Shuaijun & Wang, Shuang & Zhang, Shu & Huang, Yong & Liu, Dongjing & Wang, Qian, 2021. "Hydrogen rich syngas production from sorption enhanced gasification of cellulose in the presence of calcium oxide," Energy, Elsevier, vol. 228(C).
    6. Muniyappan, Dineshkumar & Pereira Junior, Amaro Olimpio & M, Angkayarkan Vinayakaselvi & Ramanathan, Anand, 2023. "Synergistic recovery of renewable hydrocarbon resources via microwave co-pyrolysis of biomass residue and plastic waste over spent toner catalyst towards sustainable solid waste management," Energy, Elsevier, vol. 278(C).
    7. Li, Bin & Huang, Huimin & Xie, Xing & Wei, Juntao & Zhang, Shu & Hu, Xun & Zhang, Shihong & Liu, Dongjing, 2023. "Volatile-char interactions during biomass pyrolysis: Effects of AAEMs removal and KOH addition in char," Renewable Energy, Elsevier, vol. 219(P1).
    8. Sun, Hongliang & Feng, Dongdong & Zhao, Yijun & Sun, Shaozeng, 2023. "Optimization of operating parameters for tar reforming/hydrogen upgrading in corn straw pyrolysis polygeneration," Renewable Energy, Elsevier, vol. 214(C), pages 1-10.
    9. Li, Bin & Song, Mengge & Xie, Xing & Wei, Juntao & Xu, Deliang & Ding, Kuan & Huang, Yong & Zhang, Shu & Hu, Xun & Zhang, Shihong & Liu, Dongjing, 2023. "Oxidative fast pyrolysis of biomass in a quartz tube fluidized bed reactor: Effect of oxygen equivalence ratio," Energy, Elsevier, vol. 270(C).
    10. Leng, Lijian & Li, Tanghao & Zhan, Hao & Rizwan, Muhammad & Zhang, Weijin & Peng, Haoyi & Yang, Zequn & Li, Hailong, 2023. "Machine learning-aided prediction of nitrogen heterocycles in bio-oil from the pyrolysis of biomass," Energy, Elsevier, vol. 278(PB).
    11. Qin, Liyuan & Wu, Yang & Jiang, Enchen, 2022. "In situ template preparation of porous carbon materials that are derived from swine manure and have ordered hierarchical nanopore structures for energy storage," Energy, Elsevier, vol. 242(C).
    12. Yajing He & Shihong Zhang & Dongjing Liu & Xing Xie & Bin Li, 2023. "Effect of Biomass Particle Size on the Torrefaction Characteristics in a Fixed-Bed Reactor," Energies, MDPI, vol. 16(3), pages 1-14, January.
    13. Li, Chao & Jiang, Yuchen & Shao, Yuewen & Gao, Guoming & Fan, Mengjiao & Zhang, Lijun & Zhang, Shu & Xiang, Jun & Hu, Song & Wang, Yi & Hu, Xun, 2024. "Quantification of degree of interactions during co-pyrolysis of nine typical carbonaceous wastes," Renewable Energy, Elsevier, vol. 227(C).
    14. Liu, Shasha & Wu, Gang & Gao, Yi & Li, Bin & Feng, Yu & Zhou, Jianbin & Hu, Xun & Huang, Yong & Zhang, Shu & Zhang, Hong, 2021. "Understanding the catalytic upgrading of bio-oil from pine pyrolysis over CO2-activated biochar," Renewable Energy, Elsevier, vol. 174(C), pages 538-546.

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