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Dynamic study of adsorbers by a new gravimetric version of the Large Temperature Jump method

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  • Sapienza, Alessio
  • Santamaria, Salvatore
  • Frazzica, Andrea
  • Freni, Angelo
  • Aristov, Yuri I.

Abstract

This paper presents a new experimental setup devoted to measure the ad-/desorption kinetics of an Ad-HEX (adsorbent+heat exchanger) under typical boundary conditions of an Adsorption Heat Transformer (AHT) as well as the results of the first test campaign carried out. The experimental apparatus can be considered as a gravimetric version of the known Large Temperature Jump method. In fact, the dynamic evolution of the uptake during the isobaric ad-/desorption stages is directly measured by a weighing system suitable to work in the range of 5–600g of sample mass (adsorbent+HEX) with the accuracy ±0.1g and the time response shorter than 0.1s The experimental campaign was conducted on an Ad-HEX composed of granules of a commercial SAPO-34 adsorbent placed on a flat type aluminum HEX, under operating conditions reproducing two different thermodynamic cycles (Th=90°C, Te=10°C, Tc=30 and 35°C), typical for adsorption air conditioning.

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  • Sapienza, Alessio & Santamaria, Salvatore & Frazzica, Andrea & Freni, Angelo & Aristov, Yuri I., 2014. "Dynamic study of adsorbers by a new gravimetric version of the Large Temperature Jump method," Applied Energy, Elsevier, vol. 113(C), pages 1244-1251.
    • Handle: RePEc:eee:appene:v:113:y:2014:i:c:p:1244-1251
    DOI: 10.1016/j.apenergy.2013.09.005
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    1. Chen, C.J. & Wang, R.Z. & Xia, Z.Z. & Kiplagat, J.K. & Lu, Z.S., 2010. "Study on a compact silica gel-water adsorption chiller without vacuum valves: Design and experimental study," Applied Energy, Elsevier, vol. 87(8), pages 2673-2681, August.
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    4. Choudhury, Biplab & Saha, Bidyut Baran & Chatterjee, Pradip K. & Sarkar, Jyoti Prakas, 2013. "An overview of developments in adsorption refrigeration systems towards a sustainable way of cooling," Applied Energy, Elsevier, vol. 104(C), pages 554-567.
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    6. Santamaria, Salvatore & Sapienza, Alessio & Frazzica, Andrea & Freni, Angelo & Girnik, Ilya S. & Aristov, Yuri I., 2014. "Water adsorption dynamics on representative pieces of real adsorbers for adsorptive chillers," Applied Energy, Elsevier, vol. 134(C), pages 11-19.
    7. Elsayed, Ahmed M. & Askalany, Ahmed A. & Shea, Andrew D. & Dakkama, Hassan J. & Mahmoud, Saad & Al-Dadah, Raya & Kaialy, Waseem, 2017. "A state of the art of required techniques for employing activated carbon in renewable energy powered adsorption applications," Renewable and Sustainable Energy Reviews, Elsevier, vol. 79(C), pages 503-519.
    8. Tokarev, M.M. & Aristov, Yu.I., 2017. "A new version of the Large Temperature Jump method: The thermal response (T–LTJ)," Energy, Elsevier, vol. 140(P1), pages 481-487.
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    10. Aristov, Yuri I., 2020. "Dynamics of adsorptive heat conversion systems: Review of basics and recent advances," Energy, Elsevier, vol. 205(C).
    11. Gordeeva, Larisa & Frazzica, Andrea & Sapienza, Alessio & Aristov, Yuri & Freni, Angelo, 2014. "Adsorption cooling utilizing the “LiBr/silica – ethanol” working pair: Dynamic optimization of the adsorber/heat exchanger unit," Energy, Elsevier, vol. 75(C), pages 390-399.
    12. Girnik, Ilya S. & Aristov, Yuri I., 2016. "Dynamics of water vapour adsorption by a monolayer of loose AQSOA™-FAM-Z02 grains: Indication of inseparably coupled heat and mass transfer," Energy, Elsevier, vol. 114(C), pages 767-773.
    13. Okunev, Boris N. & Aristov, Yuri I., 2014. "Making adsorptive chillers faster by a proper choice of adsorption isobar shape: Comparison of optimal and real adsorbents," Energy, Elsevier, vol. 76(C), pages 400-405.
    14. Palomba, V. & Lombardo, W. & Groβe, A. & Herrmann, R. & Nitsch, B. & Strehlow, A. & Bastian, R. & Sapienza, A. & Frazzica, A., 2020. "Evaluation of in-situ coated porous structures for hybrid heat pumps," Energy, Elsevier, vol. 209(C).
    15. Teng, W.S. & Leong, K.C. & Chakraborty, A., 2016. "Revisiting adsorption cooling cycle from mathematical modelling to system development," Renewable and Sustainable Energy Reviews, Elsevier, vol. 63(C), pages 315-332.
    16. Girnik, Ilya S. & Aristov, Yuri I., 2016. "Dynamic optimization of adsorptive chillers: The “AQSOA™-FAM-Z02 – Water” working pair," Energy, Elsevier, vol. 106(C), pages 13-22.
    17. Aristov, Yu. I., 2022. "Adsorption heat conversion and storage in closed systems: What have we learned over the past decade of this century?," Energy, Elsevier, vol. 239(PB).
    18. N'Tsoukpoe, Kokouvi Edem & Restuccia, Giovanni & Schmidt, Thomas & Py, Xavier, 2014. "The size of sorbents in low pressure sorption or thermochemical energy storage processes," Energy, Elsevier, vol. 77(C), pages 983-998.
    19. Palomba, Valeria & Sapienza, Alessio & Aristov, Yuri, 2019. "Dynamics and useful heat of the discharge stage of adsorptive cycles for long term thermal storage," Applied Energy, Elsevier, vol. 248(C), pages 299-309.
    20. Sapienza, Alessio & Velte, Andreas & Girnik, Ilya & Frazzica, Andrea & Füldner, Gerrit & Schnabel, Lena & Aristov, Yuri, 2017. "“Water - Silica Siogel” working pair for adsorption chillers: Adsorption equilibrium and dynamics," Renewable Energy, Elsevier, vol. 110(C), pages 40-46.

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