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Slow pyrolysis of Defatted Seeds Cakes of African star apple and silk cotton for production of bio-oil

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  • Sokoto, Muhammad Abdullahi
  • Biswas, Bijoy
  • Kumar, Jitendra
  • Bhaskar, Thallada

Abstract

The prospect of de-oiled seed cakes of African star apple (ASA) and Silk cotton (SCS) as a source of bio-oil was investigated using slow pyrolysis. The study was carried out at a temperatures range of 300–450 °C with a heating rate of 10 °C min−1 for 60 min residence period in a nitrogen atmosphere. The optimum bio-oil yields for SCS (33.1%) and for ASA (48.3%) were achieved at 400 °C. The Bio-char yield decreases from 300 °C to 450 °C (38%–28%) for ASA seedcake which could be due to greater primary decomposition of the biomass samples. A similar trend also observed for SCS with a lowest bio-char yield of 32% at 450 °C. The GC-MS analysis showed that ASA bio-oil has an acids (25.15%), phenolics (18.35%), and hydrocarbons (18.58%) as the major compounds. N-containg compounds (38.17%), carboxylic acid (23.79%), and phenolic (16.57%) were the dominant compounds in SCS bio-oil. The FT-IR absorption peak showed at 1660 cm−1 (C = N stretching) with higher intensity for SCS bio-oil. At optimum temperature 400 °C, 72% of ASA feedstock was converted into bio-oil and gaseous products (conversion), while 68% conversion was obtained from SCS at optimum temperature 400 °C.

Suggested Citation

  • Sokoto, Muhammad Abdullahi & Biswas, Bijoy & Kumar, Jitendra & Bhaskar, Thallada, 2020. "Slow pyrolysis of Defatted Seeds Cakes of African star apple and silk cotton for production of bio-oil," Renewable Energy, Elsevier, vol. 146(C), pages 1710-1716.
    • Handle: RePEc:eee:renene:v:146:y:2020:i:c:p:1710-1716
    DOI: 10.1016/j.renene.2019.07.145
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    References listed on IDEAS

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    1. Garg, Rahul & Anand, Neeru & Kumar, Dinesh, 2016. "Pyrolysis of babool seeds (Acacia nilotica) in a fixed bed reactor and bio-oil characterization," Renewable Energy, Elsevier, vol. 96(PA), pages 167-171.
    2. Beis, S.H. & Onay, Ö. & Koçkar, Ö.M., 2002. "Fixed-bed pyrolysis of safflower seed: influence of pyrolysis parameters on product yields and compositions," Renewable Energy, Elsevier, vol. 26(1), pages 21-32.
    3. Özbay, N & Pütün, A.E & Uzun, B.B & Pütün, E, 2001. "Biocrude from biomass: pyrolysis of cottonseed cake," Renewable Energy, Elsevier, vol. 24(3), pages 615-625.
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    2. Zalazar-Garcia, Daniela & Fernandez, Anabel & Rodriguez-Ortiz, Leandro & Torres, Erick & Reyes-Urrutia, Andrés & Echegaray, Marcelo & Rodriguez, Rosa & Mazza, Germán, 2022. "Exergo-ecological analysis and life cycle assessment of agro-wastes using a combined simulation approach based on Cape-Open to Cape-Open (COCO) and SimaPro free-software," Renewable Energy, Elsevier, vol. 201(P1), pages 60-71.

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