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Two-train elevated-temperature pressure swing adsorption for high-purity hydrogen production

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  • Zhu, Xuancan
  • Shi, Yixiang
  • Li, Shuang
  • Cai, Ningsheng

Abstract

The trade-off between hydrogen recovery ratio (HRR) and hydrogen purity (HP) is one of the main drawbacks in normal temperature pressure swing adsorption (NT-PSA) for producing high-purity hydrogen from shifted gas. In this paper, a two-train elevated-temperature pressure swing adsorption (ET-PSA) process that achieved 99.999% HP and over 95% HRR is proposed, which has wide application potentials in fuel cells and chemical industries. Potassium-promoted layered double oxide (K-LDO), which shows reasonable working capacity and fast adsorption/desorption kinetics at elevated temperatures (200–450 °C), is adopted as the CO2 adsorbent. CO in the shifted gas is co-purified by high-temperature water gas shift (WGS) catalysts added to the columns. The first-train ET-PSA adopted an eight-column thirteen-step configuration with shorter step time to remove most of the CO/CO2 in the shifted gas, and the second-train ET-PSA adopted a double-column seven-step configuration with longer step time to purify the residual gas impurities. The introduction of co-current high-pressure steam rinse and counter-current low-pressure steam purge is the key to achieve both high HRR and HP. The high-temperature steam is the main energy consumption of ET-PSA rather than low HRR in NT-PSA, and the total steam consumption is reduced by adopting the tail gas from second-train ET-PSA as the purge gas for first-train ET-PSA. The optimal results achieved 97.51% HRR and 99.9994% HP with only 0.188 rinse-to-feed ratio and 0.263 purge-to-feed ratio, which are the highest values reported for PSAs producing high-purity hydrogen from carbon-based fuels.

Suggested Citation

  • Zhu, Xuancan & Shi, Yixiang & Li, Shuang & Cai, Ningsheng, 2018. "Two-train elevated-temperature pressure swing adsorption for high-purity hydrogen production," Applied Energy, Elsevier, vol. 229(C), pages 1061-1071.
    • Handle: RePEc:eee:appene:v:229:y:2018:i:c:p:1061-1071
    DOI: 10.1016/j.apenergy.2018.08.093
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    Cited by:

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    3. Zhu, Xuancan & Ge, Tianshu & Yang, Fan & Wang, Ruzhu, 2021. "Design of steam-assisted temperature vacuum-swing adsorption processes for efficient CO2 capture from ambient air," Renewable and Sustainable Energy Reviews, Elsevier, vol. 137(C).
    4. Situmorang, Yohanes Andre & Zhao, Zhongkai & An, Ping & Yu, Tao & Rizkiana, Jenny & Abudula, Abuliti & Guan, Guoqing, 2020. "A novel system of biomass-based hydrogen production by combining steam bio-oil reforming and chemical looping process," Applied Energy, Elsevier, vol. 268(C).
    5. Casadio, Simone & Gondolini, Angela & Mercadelli, Elisa & Sanson, Alessandra, 2024. "Advances and prospects in manufacturing of ceramic oxygen and hydrogen separation membranes," Renewable and Sustainable Energy Reviews, Elsevier, vol. 200(C).
    6. Zhu, Xuancan & Chen, Chunping & Suo, Hongri & Wang, Qiang & Shi, Yixiang & O'Hare, Dermot & Cai, Ningsheng, 2019. "Synthesis of elevated temperature CO2 adsorbents from aqueous miscible organic-layered double hydroxides," Energy, Elsevier, vol. 167(C), pages 960-969.
    7. Simonas Cerniauskas & Thomas Grube & Aaron Praktiknjo & Detlef Stolten & Martin Robinius, 2019. "Future Hydrogen Markets for Transportation and Industry: The Impact of CO 2 Taxes," Energies, MDPI, vol. 12(24), pages 1-26, December.
    8. Subraveti, Sai Gokul & Pai, Kasturi Nagesh & Rajagopalan, Ashwin Kumar & Wilkins, Nicholas Stiles & Rajendran, Arvind & Jayaraman, Ambalavan & Alptekin, Gokhan, 2019. "Cycle design and optimization of pressure swing adsorption cycles for pre-combustion CO2 capture," Applied Energy, Elsevier, vol. 254(C).

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