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Solvothermal In-Situ Synthesis of MIL-53(Fe)@Carbon Felt Photocatalytic Membrane for Rhodamine B Degradation

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  • Shuyan Yu

    (School of Energy and Environmental Engineering, University of Science and Technology Beijing, Beijing 100083, China
    Beijing Key Laboratory of Resource-Oriented Treatment of Industrial Pollutants, Beijing 100083, China
    Energy Conservation and Environmental Protection Engineering Research Center in Universities of Beijing, Beijing 100083, China)

  • Huiying Zhang

    (School of Energy and Environmental Engineering, University of Science and Technology Beijing, Beijing 100083, China
    Beijing Key Laboratory of Resource-Oriented Treatment of Industrial Pollutants, Beijing 100083, China
    Energy Conservation and Environmental Protection Engineering Research Center in Universities of Beijing, Beijing 100083, China)

  • Congju Li

    (School of Energy and Environmental Engineering, University of Science and Technology Beijing, Beijing 100083, China
    Beijing Key Laboratory of Resource-Oriented Treatment of Industrial Pollutants, Beijing 100083, China
    Energy Conservation and Environmental Protection Engineering Research Center in Universities of Beijing, Beijing 100083, China)

Abstract

In this study, MIL-53(Fe) was innovatively incorporated into carbon felt (CF) by growing in-situ using the solvothermal method. MIL-53(Fe)@carbon felt (MIL-53(Fe)@CF) was prepared and used for the degradation of rhodamine B (RhB). As a new photocatalytic membrane, MIL-53(Fe)@CF photocatalytic membrane has the characteristics of high degradation efficiency and recyclability. Influence of various parameters including MIL-53(Fe)@CF loading, light, electron trapper type, and starting pH on RhB degradation were investigated. The morphology, structure, and degradation properties of MIL-53(Fe)@CF photocatalytic membrane were characterized. Corresponding reaction mechanisms were explored. The results indicated that pH at 4.5 and 1 mmol/L H 2 O 2 , 150 mg MIL-53(Fe)@CF could photocatalytically degrade 1 mg/L RhB by 98.8% within 120 min, and the reaction rate constant (k) could reach 0.03635 min −1 . The clearance rate of RhB decreased by only 2.8% after three operations. MIL-53(Fe)@CF photocatalytic membrane was found to be stable.

Suggested Citation

  • Shuyan Yu & Huiying Zhang & Congju Li, 2023. "Solvothermal In-Situ Synthesis of MIL-53(Fe)@Carbon Felt Photocatalytic Membrane for Rhodamine B Degradation," IJERPH, MDPI, vol. 20(5), pages 1-13, March.
    • Handle: RePEc:gam:jijerp:v:20:y:2023:i:5:p:4571-:d:1087750
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