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FTIR quantitative analysis technique for gases. Application in a biomass thermochemical process

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  • Granada, E.
  • Eguía, P.
  • Vilan, J.A.
  • Comesaña, J.A.
  • Comesaña, R.

Abstract

The present work proposes a novel and alternative FTIR calibration method to quantify gases. Unknown concentrations are deducted from calibration curves, obtained by combining a dilution flow with another flow of the gas of interest. Both streams are controlled by accurate flow meters. In the present case the method is used to quantify the main light gaseous products (CO, CO2 and CH4) from the pyrolysis of several biomasses. Pyrolysis is reached by thermogravimetric analysis (TGA) forming the well-known tandem TG-FTIR, relating in this way weight loss with the spectra in a given time. In addition, it has been studied the effects of parameters such as chemical composition, temperature and heating rate, on the emissions of these pyrolysis products.

Suggested Citation

  • Granada, E. & Eguía, P. & Vilan, J.A. & Comesaña, J.A. & Comesaña, R., 2012. "FTIR quantitative analysis technique for gases. Application in a biomass thermochemical process," Renewable Energy, Elsevier, vol. 41(C), pages 416-421.
    • Handle: RePEc:eee:renene:v:41:y:2012:i:c:p:416-421
    DOI: 10.1016/j.renene.2011.11.020
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    References listed on IDEAS

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    Cited by:

    1. Chhabra, Vibhuti & Bambery, Keith & Bhattacharya, Sankar & Shastri, Yogendra, 2020. "Thermal and in situ infrared analysis to characterise the slow pyrolysis of mixed municipal solid waste (MSW) and its components," Renewable Energy, Elsevier, vol. 148(C), pages 388-401.
    2. Comesaña, R. & Gómez, M.A. & Álvarez Feijoo, M.A. & Eguía, P., 2013. "CFD simulation of a TG–DSC furnace during the indium phase change process," Applied Energy, Elsevier, vol. 102(C), pages 293-298.
    3. Liu, Chao & Liu, Jingyong & Evrendilek, Fatih & Xie, Wuming & Kuo, Jiahong & Buyukada, Musa, 2020. "Bioenergy and emission characterizations of catalytic combustion and pyrolysis of litchi peels via TG-FTIR-MS and Py-GC/MS," Renewable Energy, Elsevier, vol. 148(C), pages 1074-1093.
    4. Feng, Dongdong & Zhang, Yu & Zhao, Yijun & Sun, Shaozeng, 2018. "Catalytic effects of ion-exchangeable K+ and Ca2+ on rice husk pyrolysis behavior and its gas–liquid–solid product properties," Energy, Elsevier, vol. 152(C), pages 166-177.
    5. Granada, Enrique & Míguez, J.L. & Febrero, Lara & Collazo, Joaquín & Eguía, Pablo, 2013. "Development of an experimental technique for oil recovery during biomass pyrolysis," Renewable Energy, Elsevier, vol. 60(C), pages 179-184.

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