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Influence of vacuum degree on hydrogen permeation through a Pd membrane in different H2/N2 gas mixtures

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  • Chen, Wei-Hsin
  • Escalante, Jamin

Abstract

Palladium (Pd) membranes for industrial applications have gained much interest as of late. The purification of hydrogen through Pd membranes has therefore been proposed as a viable solution to traditional separation methods. Hydrogen permeation can be enhanced when coupled with a vacuum at the permeate side. In this study, the effect of different degrees of vacuum pressures on H2 permeation through a high-permselectivity Pd membrane in different binary gas mixtures was investigated and compared to those without vacuum. Three feed gases containing H2 concentrations of 90, 70, and 50 vol% were used. Hydrogen permeation rates were studied at 320, 350, and 380 °C under vacuum pressures ranging between 0 and −60 kPa. An increase in vacuum degree intensified H2 permeation. However, best performance improvements were observed at lower H2 concentrations, lower temperatures, and also at lower vacuum pressures for all gas mixtures. The highest performance improvement of 88.83% was with the gas mixture containing 50% H2 at 320 °C with a −15 kPa vacuum pressure. Hence, from an efficiency point of view, lower temperatures and vacuum pressures were preferred for all the gas mixtures. Activation Energies were also relatively lower for conditions with a vacuum for all gas mixtures.

Suggested Citation

  • Chen, Wei-Hsin & Escalante, Jamin, 2020. "Influence of vacuum degree on hydrogen permeation through a Pd membrane in different H2/N2 gas mixtures," Renewable Energy, Elsevier, vol. 155(C), pages 1245-1263.
  • Handle: RePEc:eee:renene:v:155:y:2020:i:c:p:1245-1263
    DOI: 10.1016/j.renene.2020.04.048
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    References listed on IDEAS

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    1. Chen, Wei-Hsin & Hsia, Ming-Hsien & Chi, Yen-Hsun & Lin, Yu-Li & Yang, Chang-Chung, 2014. "Polarization phenomena of hydrogen-rich gas in high-permeance Pd and Pd–Cu membrane tubes," Applied Energy, Elsevier, vol. 113(C), pages 41-50.
    2. Chen, Wei-Hsin & Shen, Chun-Ting & Lin, Bo-Jhih & Liu, Shih-Chun, 2015. "Hydrogen production from methanol partial oxidation over Pt/Al2O3 catalyst with low Pt content," Energy, Elsevier, vol. 88(C), pages 399-407.
    3. Al-Mufachi, N.A. & Rees, N.V. & Steinberger-Wilkens, R., 2015. "Hydrogen selective membranes: A review of palladium-based dense metal membranes," Renewable and Sustainable Energy Reviews, Elsevier, vol. 47(C), pages 540-551.
    4. Shafiee, Shahriar & Topal, Erkan, 2009. "When will fossil fuel reserves be diminished?," Energy Policy, Elsevier, vol. 37(1), pages 181-189, January.
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    1. Kim, Tae-Woo & Lee, Eun-Han & Byun, Segi & Seo, Doo-Won & Hwang, Hyo-Jung & Yoon, Hyung-Chul & Kim, Hansung & Ryi, Shin-Kun, 2022. "Highly selective Pd composite membrane on porous metal support for high-purity hydrogen production through effective ammonia decomposition," Energy, Elsevier, vol. 260(C).

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