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Pretreatment of quinoa straw with 1-butyl-3-methylimidazolium chloride and physiochemical characterization of biomass

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  • Xie, Wei
  • Ren, Yanjing
  • Jiang, Fan
  • Liang, Jibao
  • Du, Shuang-kui

Abstract

Quinoa straw was pretreated with 1-butyl-3-methylimidazolium chloride ([Bmim]Cl). The levels of pretreatment temperature, duration, and liquid/solid ratio were optimized using orthogonal design to enhance the reducing sugar yield of treated sample. Scanning electron microscopy, Fourier transform infrared spectroscopy, and X-ray diffraction were used to assess structural changes in native and pretreated biomass. The effect of [Bmim]Cl pretreatment on the structure and properties of quinoa straw was significant. The optimum pretreatment conditions were liquid/solid ratio of 15:1, temperature of 100 °C, and duration of 5 h. The maximum reducing sugar yield of 33.22% was obtained, which was significantly higher than that of native quinoa straw. Unlike the untreated one, the pretreated quinoa straw showed clear pores and cracks and incomplete structure. Significant differences in the reducing sugar yield and structural characterization between [Bmim]Cl pretreated and untreated biomass demonstrated that [Bmim]Cl pretreatment of quinoa straw was effective for enzymatic hydrolysis.

Suggested Citation

  • Xie, Wei & Ren, Yanjing & Jiang, Fan & Liang, Jibao & Du, Shuang-kui, 2020. "Pretreatment of quinoa straw with 1-butyl-3-methylimidazolium chloride and physiochemical characterization of biomass," Renewable Energy, Elsevier, vol. 146(C), pages 1364-1371.
    • Handle: RePEc:eee:renene:v:146:y:2020:i:c:p:1364-1371
    DOI: 10.1016/j.renene.2019.07.072
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    References listed on IDEAS

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    1. Xie, Wei & Zhou, Dayun & Ren, Yanjing & Tang, Shurong & Kuang, Meng & Du, Shuang-kui, 2018. "1-Butyl-3-methylimidazolium chloride pretreatment of cotton stalk and structure characterization," Renewable Energy, Elsevier, vol. 125(C), pages 668-674.
    2. Nanda, Sonil & Azargohar, Ramin & Dalai, Ajay K. & Kozinski, Janusz A., 2015. "An assessment on the sustainability of lignocellulosic biomass for biorefining," Renewable and Sustainable Energy Reviews, Elsevier, vol. 50(C), pages 925-941.
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    2. Cao, Jing & Yang, Jian & Yang, Yishuo & Wang, Zhaomei, 2021. "Enhanced enzymatic hydrolysis of sisal waste by sequential pretreatment with UV-catalyzed alkaline hydrogen peroxide and ionic liquid," Renewable Energy, Elsevier, vol. 169(C), pages 1157-1165.
    3. Aghili Mehrizi, Amirreza & Tangestaninejad, Shahram & Denayer, Joeri F.M. & Karimi, Keikhosro & Shafiei, Marzieh, 2023. "The critical impacts of anion and cosolvent on morpholinium ionic liquid pretreatment for efficient renewable energy production from triticale straw," Renewable Energy, Elsevier, vol. 202(C), pages 686-698.

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