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1-Butyl-3-methylimidazolium chloride pretreatment of cotton stalk and structure characterization

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  • Xie, Wei
  • Zhou, Dayun
  • Ren, Yanjing
  • Tang, Shurong
  • Kuang, Meng
  • Du, Shuang-kui

Abstract

Cotton stalk was pretreated with 1-butyl-3-methyimidazolium chloride ([Bmim]Cl) and the effect of pretreatment factors, including liquid/solid ratio, temperature, and pretreatment duration on cotton stalk was investigated. Scanning electronic microscopy, Fourier transform infrared spectroscopy, and X-ray diffraction were used to identify structural changes in native and pretreated biomass. The optimum pretreatment conditions were as follows: liquid/solid ratio of 10:1, reaction temperature of 120 °C and duration of 5 h.The reducing sugar yield was 29.72%, which was significantly higher than that of native cotton stalk. The differences in the reducing sugar yields between [Bmim]Cl-pretreated and untreated biomass suggested that [Bmim]Cl pretreatment was effective to produce reducing sugars. The pretreated cotton stalk showed clear pores and cracks, low crystallinity, and incomplete crystal structure compared with untreated one. [Bmim]Cl could be reused at least four times without significant reduction in the reducing sugar yield.

Suggested Citation

  • Xie, Wei & Zhou, Dayun & Ren, Yanjing & Tang, Shurong & Kuang, Meng & Du, Shuang-kui, 2018. "1-Butyl-3-methylimidazolium chloride pretreatment of cotton stalk and structure characterization," Renewable Energy, Elsevier, vol. 125(C), pages 668-674.
    • Handle: RePEc:eee:renene:v:125:y:2018:i:c:p:668-674
    DOI: 10.1016/j.renene.2018.03.011
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    References listed on IDEAS

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    1. Vancov, Tony & Alston, Amy-Sue & Brown, Trevor & McIntosh, Shane, 2012. "Use of ionic liquids in converting lignocellulosic material to biofuels," Renewable Energy, Elsevier, vol. 45(C), pages 1-6.
    2. Zhang, Quanguo & Hu, Jianjun & Lee, Duu-Jong, 2017. "Pretreatment of biomass using ionic liquids: Research updates," Renewable Energy, Elsevier, vol. 111(C), pages 77-84.
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    1. Xie, Wei & Ren, Yanjing & Jiang, Fan & Liang, Jibao & Du, Shuang-kui, 2020. "Pretreatment of quinoa straw with 1-butyl-3-methylimidazolium chloride and physiochemical characterization of biomass," Renewable Energy, Elsevier, vol. 146(C), pages 1364-1371.
    2. Aghili Mehrizi, Amirreza & Tangestaninejad, Shahram & Denayer, Joeri F.M. & Karimi, Keikhosro & Shafiei, Marzieh, 2023. "The critical impacts of anion and cosolvent on morpholinium ionic liquid pretreatment for efficient renewable energy production from triticale straw," Renewable Energy, Elsevier, vol. 202(C), pages 686-698.
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