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Effect of Crambe abyssinica oil degumming in phosphorus concentration of refined oil and derived biodiesel

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  • Costa, Emanuel
  • Almeida, Manuel Fonseca
  • Alvim-Ferraz, Maria da Conceição
  • Dias, Joana Maia

Abstract

In the present study, the effect of different degumming processes on the phosphorus content of Crambe abyssinica oil and resultant biodiesel was evaluated. The non-edible oil was submitted to water degumming and chemical degumming with different concentrations of phosphoric acid and varying the acid to oil volume percentages. Phosphorus content of the products was measured by UV spectroscopy after sample calcination, according to NP 1994:2000. Biodiesel was produced by transesterification using a 6:1 methanol to oil molar ratio and 1 wt% sodium hydroxide as catalyst at 65 °C, during 1 h. The biodiesel produced directly from the crude oil presented high phosphorus concentration (>20 ppm); consequently, a degumming process was required to fulfil the quality standard (<4 ppm according to EN 14214). Water degumming was not effective, leading to biodiesel with a phosphorus concentration of 12.2 ppm. Among the acid degumming processes evaluated and taking into account technical and operational variables, the best established conditions, which allowed the fulfilment of the quality standard regarding phosphorus concentration, was considered to be 25 wt% acid concentration and 0.80 vol% of acid to oil.

Suggested Citation

  • Costa, Emanuel & Almeida, Manuel Fonseca & Alvim-Ferraz, Maria da Conceição & Dias, Joana Maia, 2018. "Effect of Crambe abyssinica oil degumming in phosphorus concentration of refined oil and derived biodiesel," Renewable Energy, Elsevier, vol. 124(C), pages 27-33.
    • Handle: RePEc:eee:renene:v:124:y:2018:i:c:p:27-33
    DOI: 10.1016/j.renene.2017.08.089
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    1. Atabani, A.E. & Silitonga, A.S. & Ong, H.C. & Mahlia, T.M.I. & Masjuki, H.H. & Badruddin, Irfan Anjum & Fayaz, H., 2013. "Non-edible vegetable oils: A critical evaluation of oil extraction, fatty acid compositions, biodiesel production, characteristics, engine performance and emissions production," Renewable and Sustainable Energy Reviews, Elsevier, vol. 18(C), pages 211-245.
    2. Diana da Silva Araújo, Francisca & Araújo, Iranildo C. & Costa, Isabella Cristhina G. & Rodarte de Moura, Carla Verônica & Chaves, Mariana H. & Araújo, Eugênio Celso E., 2014. "Study of degumming process and evaluation of oxidative stability of methyl and ethyl biodiesel of Jatropha curcas L. oil from three different Brazilian states," Renewable Energy, Elsevier, vol. 71(C), pages 495-501.
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    2. Mousavi-Avval, Seyed Hashem & Shah, Ajay, 2021. "Techno-economic analysis of hydroprocessed renewable jet fuel production from pennycress oilseed," Renewable and Sustainable Energy Reviews, Elsevier, vol. 149(C).
    3. Arora, Amit & Singh, Vijay, 2020. "Biodiesel production from engineered sugarcane lipids under uncertain feedstock compositions: Process design and techno-economic analysis," Applied Energy, Elsevier, vol. 280(C).

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