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Synthesis and optimization of Hydnocarpus wightiana and dairy waste scum as feed stock for biodiesel production by using response surface methodology

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  • Krishnamurthy, K.N.
  • Sridhara, S.N.
  • Ananda Kumar, C.S.

Abstract

This study examines that a non-edible dairy waste scum and Hydnocarpus Wightiana oil is claimed to be a highly potential feed stock for biodiesel production. Response Surface Methodology (RSM) in aggregation with Central Composite Design (CCD) is employed to evaluate the best potential combination of catalyst concentration, methanol to oil molar ratio, reaction time and temperature for higher yield of biodiesel content. A statistical model predicted that the highest conversion yield of scum oil methyl ester (SOME) and Hydnocarpus Wightiana oil methyl ester (HWOME) would be 91.636% and 94.091% at the following optimized reaction conditions: Methanol to oil molar ratio of 7.5:1 and 6.526:1, Catalyst Concentration of 0.961 wt% and 0.934 wt%, Reaction Time 49.529 min and 45 min and temperature 63.46 °C and 64.386 °C respectively. Experiments were conducted for SOME and HWOME at the predicted optimum conditions in three independent replicates, an average biodiesel yield of 90.89 ± 5% and 93.68 ± 4% was achieved which was in reasonable agreement with the predicted value. This study shows that the quality of biodiesel production from SOME and HWOME at optimum process conditions satisfies the ASTM D-6751 and EN14214 Standards. The physio-chemical properties of SOME and HWOME were determined and compared with that of diesel.

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  • Krishnamurthy, K.N. & Sridhara, S.N. & Ananda Kumar, C.S., 2018. "Synthesis and optimization of Hydnocarpus wightiana and dairy waste scum as feed stock for biodiesel production by using response surface methodology," Energy, Elsevier, vol. 153(C), pages 1073-1086.
    • Handle: RePEc:eee:energy:v:153:y:2018:i:c:p:1073-1086
    DOI: 10.1016/j.energy.2018.04.068
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    1. Singh, Yashvir & Sharma, Abhishek & Tiwari, Sumit & Singla, Amneesh, 2019. "Optimization of diesel engine performance and emission parameters employing cassia tora methyl esters-response surface methodology approach," Energy, Elsevier, vol. 168(C), pages 909-918.
    2. Krishnamurthy, K.N. & Sridhara, S.N. & Ananda Kumar, C.S., 2020. "Optimization and kinetic study of biodiesel production from Hydnocarpus wightiana oil and dairy waste scum using snail shell CaO nano catalyst," Renewable Energy, Elsevier, vol. 146(C), pages 280-296.
    3. Yatish, K.V. & Omkaresh, B.R. & Kattimani, Veeranna R. & Lalithamba, H.S. & Sakar, M. & Balakrishna, R. Geetha, 2023. "Solar energy-assisted reactor for the sustainable biodiesel production from Butea monosperma oil: Optimization, kinetic, thermodynamic and assessment studies," Energy, Elsevier, vol. 263(PB).
    4. Elkelawy, Medhat & Etaiw, Safaa El-din H. & Alm-Eldin Bastawissi, Hagar & Ayad, Mohamed I. & Radwan, Ahmed Mohamed & Dawood, Mohamed M., 2021. "Diesel/ biodiesel /silver thiocyanate nanoparticles/hydrogen peroxide blends as new fuel for enhancement of performance, combustion, and Emission characteristics of a diesel engine," Energy, Elsevier, vol. 216(C).
    5. Alvarez Serafini, Mariana S. & Reinoso, Deborath M. & Tonetto, Gabriela M., 2018. "Response surface study and kinetic modelling of biodiesel synthesis catalyzed by zinc stearate," Energy, Elsevier, vol. 164(C), pages 264-274.

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