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Parametric optimization of biodiesel synthesis from rubber seed oil using iron doped carbon catalyst by Taguchi approach

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  • Dhawane, Sumit H.
  • Bora, Akash Pratim
  • Kumar, Tarkeshwar
  • Halder, Gopinath

Abstract

Improvisation of the biodiesel production by employing heterogeneous catalyst and its optimization is the best way to mitigate the growing concern with the traditional feedstocks and their prices. The present study is aimed at optimizing the biodiesel production process and identifying significant parameters affecting the biodiesel yield. The biodiesel is synthesized from rubber seed oil (RSO) using indigenously prepared iron doped catalyst (Fe/C). The optimized condition obtained by maximizing the RSME (Rubber seed oil methyl ester) yield at 97.5% are catalyst loading 4.5 wt%, Methanol/Oil (M/O) 9:1, temperature 60 °C and agitation speed 1250 RPM. The physicochemical properties of RSME produced at optimized condition are found to be within the prescribed limits suggested by ASTM. The contribution factor estimated for individual parameters revealed that temperature, agitation speed, and M/O ratio have a more significant effect on the RSME yield. The reusability of the Fe/C catalyst was also studied to check its activity in the reuse and found to be effective after three cycles with appreciable catalytic activity. Hence, the study reveals RSO could be effective feedstock for the production of biodiesel using novel Fe/C catalyst to produce energy efficient and cost effective RSME towards the production of sustainable energy.

Suggested Citation

  • Dhawane, Sumit H. & Bora, Akash Pratim & Kumar, Tarkeshwar & Halder, Gopinath, 2017. "Parametric optimization of biodiesel synthesis from rubber seed oil using iron doped carbon catalyst by Taguchi approach," Renewable Energy, Elsevier, vol. 105(C), pages 616-624.
    • Handle: RePEc:eee:renene:v:105:y:2017:i:c:p:616-624
    DOI: 10.1016/j.renene.2016.12.096
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    References listed on IDEAS

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    1. Dhawane, Sumit H. & Kumar, Tarkeshwar & Halder, Gopinath, 2016. "Biodiesel synthesis from Hevea brasiliensis oil employing carbon supported heterogeneous catalyst: Optimization by Taguchi method," Renewable Energy, Elsevier, vol. 89(C), pages 506-514.
    2. Melvin Jose, D.F. & Edwin Raj, R. & Durga Prasad, B. & Robert Kennedy, Z. & Mohammed Ibrahim, A., 2011. "A multi-variant approach to optimize process parameters for biodiesel extraction from rubber seed oil," Applied Energy, Elsevier, vol. 88(6), pages 2056-2063, June.
    3. Atabani, A.E. & Silitonga, A.S. & Badruddin, Irfan Anjum & Mahlia, T.M.I. & Masjuki, H.H. & Mekhilef, S., 2012. "A comprehensive review on biodiesel as an alternative energy resource and its characteristics," Renewable and Sustainable Energy Reviews, Elsevier, vol. 16(4), pages 2070-2093.
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