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Esterification of jatropha oil via ultrasonic irradiation with auto-induced temperature-rise effect

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  • Andrade-Tacca, Cesar Augusto
  • Chang, Chia-Chi
  • Chen, Yi-Hung
  • Manh, Do-Van
  • Chang, Ching-Yuan
  • Ji, Dar-Ren
  • Tseng, Jyi-Yeong
  • Shie, Je-Lueng

Abstract

Auto-induced temperature-rise effects of ultrasonic irradiation (UI) on the esterification performance of jatropha oil (JO) were studied. Comparisons with other methods of mechanical mixing (MM) and hand shaking mixing were made. Major system parameters examined include: esterification time (tE), settling time (tS) after esterification and temperature. Properties of acid value (AV), iodine value (IV), kinematic viscosity (KV) and density of JO and ester product were measured. The esterification conversion efficiencies (η) were determined and assessed. Sulfuric acid was used to catalyze the esterification using methyl alcohol. For esterification without temperature control, η at tE = 10 and 30 min for UI of 56.73 and 83.23% are much higher than those for MM of 36.76 and 42.48%, respectively. At tE = 10 min, the jatropha oil esters produced via UI and MM respectively possess AV of 15.82 and 23.12 mg KOH/g, IV of 111.49 and 113.22 g I2/100g, KV of 22.41 and 22.51 mm2/s and density of 913.8 and 913.58 kg/m3, showing that UI is much better than MM in enhancing the reduction of AV. The tE exhibits more vigorous effect on AV for UI than MM. The UI offers auto-induced temperature-rise, improving the mixing and esterification extents.

Suggested Citation

  • Andrade-Tacca, Cesar Augusto & Chang, Chia-Chi & Chen, Yi-Hung & Manh, Do-Van & Chang, Ching-Yuan & Ji, Dar-Ren & Tseng, Jyi-Yeong & Shie, Je-Lueng, 2014. "Esterification of jatropha oil via ultrasonic irradiation with auto-induced temperature-rise effect," Energy, Elsevier, vol. 71(C), pages 346-354.
    • Handle: RePEc:eee:energy:v:71:y:2014:i:c:p:346-354
    DOI: 10.1016/j.energy.2014.04.066
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    1. Manh, Do-Van & Chen, Yi-Hung & Chang, Chia-Chi & Chang, Ching-Yuan & Hanh, Hoang-Duc & Chau, Nguyen-Hoai & Tuyen, Trinh-Van & Long, Pham-Quoc & Minh, Chau-Van, 2012. "Effects of blending composition of tung oil and ultrasonic irradiation intensity on the biodiesel production," Energy, Elsevier, vol. 48(1), pages 519-524.
    2. Jain, Siddharth & Sharma, M.P., 2010. "Biodiesel production from Jatropha curcas oil," Renewable and Sustainable Energy Reviews, Elsevier, vol. 14(9), pages 3140-3147, December.
    3. Chen, Yi-Hung & Chen, Jhih-Hong & Luo, Yu-Min & Shang, Neng-Chou & Chang, Cheng-Hsin & Chang, Ching-Yuan & Chiang, Pen-Chi & Shie, Je-Lueng, 2011. "Property modification of jatropha oil biodiesel by blending with other biodiesels or adding antioxidants," Energy, Elsevier, vol. 36(7), pages 4415-4421.
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    Cited by:

    1. Chia-Chi Chang & Syuan Teng & Min-Hao Yuan & Dar-Ren Ji & Ching-Yuan Chang & Yi-Hung Chen & Je-Lueng Shie & Chungfang Ho & Sz-Ying Tian & Cesar Augusto Andrade-Tacca & Do Van Manh & Min-Yi Tsai & Mei-, 2018. "Esterification of Jatropha Oil with Isopropanol via Ultrasonic Irradiation," Energies, MDPI, vol. 11(6), pages 1-15, June.
    2. Yi-Yu Wang & Chia-Chi Chang & Ching-Yuan Chang & Yi-Hung Chen & Je-Lueng Shie & Min-Hao Yuan & Yen-Hau Chen & Li-Xuan Huang & Cesar Augusto Andrade-Tacca & Do Van Manh & Min-Yi Tsai & Michael Huang, 2016. "Thermal Cracking of Jatropha Oil with Hydrogen to Produce Bio-Fuel Oil," Energies, MDPI, vol. 9(11), pages 1-11, November.
    3. Gollakota, Anjani R.K. & Reddy, Madhurima & Subramanyam, Malladi D. & Kishore, Nanda, 2016. "A review on the upgradation techniques of pyrolysis oil," Renewable and Sustainable Energy Reviews, Elsevier, vol. 58(C), pages 1543-1568.

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