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Two-Stage Continuous Process for the Extraction of Silica from Rice Husk Using Attrition Ball Milling and Alkaline Leaching Methods

Author

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  • Ji Yeon Park

    (Korea Institute of Ceramic Engineering and Technology (KICET), Heungdeok-gu, Cheongju-si 28160, Korea
    Division of Chemical Engineering & Bio Engineering, Hanyang University, Seoul 04763, Korea)

  • Yang Mo Gu

    (Korea Institute of Ceramic Engineering and Technology (KICET), Heungdeok-gu, Cheongju-si 28160, Korea
    Division of Chemical Engineering & Bio Engineering, Hanyang University, Seoul 04763, Korea)

  • Seon Young Park

    (Korea Institute of Ceramic Engineering and Technology (KICET), Heungdeok-gu, Cheongju-si 28160, Korea
    Division of Chemical Engineering & Bio Engineering, Hanyang University, Seoul 04763, Korea)

  • Ee Taek Hwang

    (Department of Food Biotechnology, Dong-A University, Busan 49315, Korea)

  • Byoung-In Sang

    (Division of Chemical Engineering & Bio Engineering, Hanyang University, Seoul 04763, Korea)

  • Jinyoung Chun

    (Korea Institute of Ceramic Engineering and Technology (KICET), Heungdeok-gu, Cheongju-si 28160, Korea)

  • Jin Hyung Lee

    (Korea Institute of Ceramic Engineering and Technology (KICET), Heungdeok-gu, Cheongju-si 28160, Korea)

Abstract

A two-stage continuous process was developed for improved silica extraction from rice husk. The two-stage continuous process consists of attrition ball milling and alkaline leaching methods. To find the optimum conditions for the continuous process, the effects of alkaline leaching parameters, such as the alkaline solution type and reaction conditions, on the silica extraction yield were investigated in a batch process. The use of NaOH showed a slightly higher silica yield than KOH. The optimum reaction conditions were found to be 0.2 M, 80 °C, 3 h, and 6% ( w / v ) for the reaction concentration, temperature, duration time, and solid content, respectively. Attrition ball milling was used to make micron-sized rice husk particles and to improve the fluidity of the rice husk slurry. The two-stage continuous process was performed using optimum conditions as determined based on the results of the batch experiment. The two-stage continuous extraction was stably operated for 80 h with an 89% silica yield. During the operation, the solid content remained consistent at 6% ( w / v ). The obtained silica was characterized using inductively coupled plasma–optical emission spectrometry (ICP–OES), X-ray diffraction (XRD), and the Brunauer–Emmett–Teller (BET) method.

Suggested Citation

  • Ji Yeon Park & Yang Mo Gu & Seon Young Park & Ee Taek Hwang & Byoung-In Sang & Jinyoung Chun & Jin Hyung Lee, 2021. "Two-Stage Continuous Process for the Extraction of Silica from Rice Husk Using Attrition Ball Milling and Alkaline Leaching Methods," Sustainability, MDPI, vol. 13(13), pages 1-11, June.
    • Handle: RePEc:gam:jsusta:v:13:y:2021:i:13:p:7350-:d:586084
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    References listed on IDEAS

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    1. Jinyoung Chun & Jin Hyung Lee, 2020. "Recent Progress on the Development of Engineered Silica Particles Derived from Rice Husk," Sustainability, MDPI, vol. 12(24), pages 1-19, December.
    2. Pode, Ramchandra, 2016. "Potential applications of rice husk ash waste from rice husk biomass power plant," Renewable and Sustainable Energy Reviews, Elsevier, vol. 53(C), pages 1468-1485.
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