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Toward Complete Utilization of Miscanthus in a Hot-Water Extraction-Based Biorefinery

Author

Listed:
  • Kuo-Ting Wang

    (Department of Paper and Bioprocess Engineering, SUNY College of Environmental Science and Forestry, 1 Forestry Drive, Syracuse, NY 13210, USA)

  • Chengyan Jing

    (Department of Paper and Bioprocess Engineering, SUNY College of Environmental Science and Forestry, 1 Forestry Drive, Syracuse, NY 13210, USA)

  • Christopher Wood

    (Department of Paper and Bioprocess Engineering, SUNY College of Environmental Science and Forestry, 1 Forestry Drive, Syracuse, NY 13210, USA)

  • Aditi Nagardeolekar

    (Department of Paper and Bioprocess Engineering, SUNY College of Environmental Science and Forestry, 1 Forestry Drive, Syracuse, NY 13210, USA)

  • Neil Kohan

    (Department of Paper and Bioprocess Engineering, SUNY College of Environmental Science and Forestry, 1 Forestry Drive, Syracuse, NY 13210, USA)

  • Prajakta Dongre

    (Department of Paper and Bioprocess Engineering, SUNY College of Environmental Science and Forestry, 1 Forestry Drive, Syracuse, NY 13210, USA)

  • Thomas E. Amidon

    (Department of Paper and Bioprocess Engineering, SUNY College of Environmental Science and Forestry, 1 Forestry Drive, Syracuse, NY 13210, USA)

  • Biljana M. Bujanovic

    (Department of Paper and Bioprocess Engineering, SUNY College of Environmental Science and Forestry, 1 Forestry Drive, Syracuse, NY 13210, USA)

Abstract

Miscanthus ( Miscanthus sp. Family: Poaceae ) was hot-water extracted (two h, at 160 °C) at three scales: laboratory (Parr reactor, 300 cm 3 ), intermediate (M/K digester, 4000 cm 3 ), and pilot (65 ft 3 -digester, 1.841 × 10 6 cm 3 ). Hot-water extracted miscanthus, hydrolyzate, and lignin recovered from hydrolyzate were characterized and evaluated for potential uses aiming at complete utilization of miscanthus. Effects of scale-up on digester yield, removal of hemicelluloses, deashing, delignification degree, lignin recovery and purity, and cellulose retention were studied. The scale-dependent results demonstrated that before implementation, hot-water extraction (HWE) should be evaluated on a scale larger than a laboratory scale. The production of energy-enriched fuel pellets from hot-water extracted miscanthus, especially in combination with recovered lignin is recommended, as energy of combustion increased gradually from native to hot-water extracted miscanthus to recovered lignin. The native and pilot-scale hot-water extracted miscanthus samples were also subjected to enzymatic hydrolysis using a cellulase-hemicellulase cocktail, to produce fermentable sugars. Hot-water extracted biomass released higher amount of glucose and xylose verifying benefits of HWE as an effective pretreatment for xylan-rich lignocellulosics. The recovered lignin was used to prepare a formaldehyde-free alternative to phenol-formaldehyde resins and as an antioxidant. Promising results were obtained for these lignin valorization pathways.

Suggested Citation

  • Kuo-Ting Wang & Chengyan Jing & Christopher Wood & Aditi Nagardeolekar & Neil Kohan & Prajakta Dongre & Thomas E. Amidon & Biljana M. Bujanovic, 2017. "Toward Complete Utilization of Miscanthus in a Hot-Water Extraction-Based Biorefinery," Energies, MDPI, vol. 11(1), pages 1-22, December.
    • Handle: RePEc:gam:jeners:v:11:y:2017:i:1:p:39-:d:124286
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    References listed on IDEAS

    as
    1. Chen Gong & Biljana M. Bujanovic, 2014. "Impact of Hot-Water Extraction on Acetone-Water Oxygen Delignification of Paulownia Spp. and Lignin Recovery," Energies, MDPI, vol. 7(2), pages 1-17, February.
    2. Ahn, Byoung Jun & Chang, Hee-sun & Lee, Soo Min & Choi, Don Ha & Cho, Seong Taek & Han, Gyu-seong & Yang, In, 2014. "Effect of binders on the durability of wood pellets fabricated from Larix kaemferi C. and Liriodendron tulipifera L. sawdust," Renewable Energy, Elsevier, vol. 62(C), pages 18-23.
    3. Xu, Jian & Liu, Shijie, 2009. "Optimization of ethanol production from hot-water extracts of sugar maple chips," Renewable Energy, Elsevier, vol. 34(11), pages 2353-2356.
    4. Prajakta Dongre & Mark Driscoll & Thomas Amidon & Biljana Bujanovic, 2015. "Lignin-Furfural Based Adhesives," Energies, MDPI, vol. 8(8), pages 1-18, July.
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    Cited by:

    1. Christopher D. Wood & Thomas E. Amidon & Timothy A. Volk & Rachel M. Emerson, 2020. "Hot Water Extraction: Short Rotation Willow, Mixed Hardwoods, and Process Considerations," Energies, MDPI, vol. 13(8), pages 1-20, April.

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