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Esterification of lauric acid with butanol over mesoporous materials

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  • Barros, Suellen D.T.
  • Coelho, Aline V.
  • Lachter, Elizabeth R.
  • San Gil, Rosane A.S.
  • Dahmouche, Karim
  • Pais da Silva, Maria Isabel
  • Souza, Andrea L.F.

Abstract

Mesoporous silica (e.g. SBA-15) was evaluated in the esterification of lauric acid with butanol. ZnO/SBA-15 and MgO/SBA-15 were synthesized and characterized using N2 adsorption/desorption isotherms at 77 K, 29Si magic angle spinning solid state nuclear magnetic resonance (29Si MAS NMR), X-ray diffraction (XRD) and Small-Angle X-ray scattering (SAXS). The nanostructural parameters obtained from SAXS analysis were very similar for all samples revealing that the impregnation method for incorporation of Zn and Mg in mesoporous silica did not affect its structure. Both catalysts ZnO/SBA-15 and MgO/SBA-15 were able to promote the esterification reaction of lauric acid with 1-butanol at mild reactions conditions.

Suggested Citation

  • Barros, Suellen D.T. & Coelho, Aline V. & Lachter, Elizabeth R. & San Gil, Rosane A.S. & Dahmouche, Karim & Pais da Silva, Maria Isabel & Souza, Andrea L.F., 2013. "Esterification of lauric acid with butanol over mesoporous materials," Renewable Energy, Elsevier, vol. 50(C), pages 585-589.
    • Handle: RePEc:eee:renene:v:50:y:2013:i:c:p:585-589
    DOI: 10.1016/j.renene.2012.06.059
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    References listed on IDEAS

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    1. Hanh, Hoang Duc & Dong, Nguyen The & Okitsu, Kenji & Nishimura, Rokuro & Maeda, Yasuaki, 2009. "Biodiesel production by esterification of oleic acid with short-chain alcohols under ultrasonic irradiation condition," Renewable Energy, Elsevier, vol. 34(3), pages 780-783.
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    1. Kaur, Navjot & Ali, Amjad, 2015. "Preparation and application of Ce/ZrO2−TiO2/SO42− as solid catalyst for the esterification of fatty acids," Renewable Energy, Elsevier, vol. 81(C), pages 421-431.
    2. Rezende, Michelle J.C. & Pinto, Angelo C., 2016. "Esterification of fatty acids using acid-activated Brazilian smectite natural clay as a catalyst," Renewable Energy, Elsevier, vol. 92(C), pages 171-177.
    3. Mauro Banchero & Giuseppe Gozzelino, 2018. "A Simple Pseudo-Homogeneous Reversible Kinetic Model for the Esterification of Different Fatty Acids with Methanol in the Presence of Amberlyst-15," Energies, MDPI, vol. 11(7), pages 1-12, July.
    4. de Aguiar, Viviane Marques & de Souza, Andrea Luzia F. & Galdino, Fernanda S. & da Silva, Michelle Martha C. & Teixeira, Viviane Gomes & Lachter, Elizabeth R., 2017. "Sulfonated poly(divinylbenzene) and poly(styrene-divinylbenzene) as catalysts for esterification of fatty acids," Renewable Energy, Elsevier, vol. 114(PB), pages 725-732.

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