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Understanding the nature of bio-asphaltenes produced during hydrothermal liquefaction

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  • Robertson, Gilles
  • Adiningtyas, Kusuma Virginna
  • Ebrahim, Sayed Ahmed
  • Scoles, Ludmila
  • Baranova, Elena A.
  • Singh, Devinder

Abstract

Asphaltenes, the heaviest and most polar components of crudes, are generally associated with considerable operational issues in refineries. In order to understand potential operational issues during upgrading/processing of bio-crudes, structural and thermal behaviour of asphaltenes derived from bio-crude (bio-asphaltenes) from hydrothermal liquefaction of food-waste and wood residues were compared with petroleum derived asphaltenes derived from bitumen. Structural analysis using nuclear magnetic resonance and elemental analysis revealed 7 aromatic rings per unit structure for bitumen asphaltenes, 4 for food-waste asphaltenes, and 3 for wood asphaltenes. The calculated molecular weight per unit structure followed the order: bitumen asphaltenes (589–636 g mol−1) > food-waste derived asphaltenes (338–358 g mol−1)> wood residue derived asphaltenes (268–274 g mol−1). The carbon residues using thermal gravimetric analysis (bitumen asphaltenes = 40%, bio-asphaltenes = 19–25%) and glass transition temperature (bitumen asphaltenes = 80 °C, bio-asphaltenes = 4–64 °C) followed the same order. These results indicate a very different structural and thermal behaviour for petroleum and bio-asphaltenes.

Suggested Citation

  • Robertson, Gilles & Adiningtyas, Kusuma Virginna & Ebrahim, Sayed Ahmed & Scoles, Ludmila & Baranova, Elena A. & Singh, Devinder, 2021. "Understanding the nature of bio-asphaltenes produced during hydrothermal liquefaction," Renewable Energy, Elsevier, vol. 173(C), pages 128-140.
    • Handle: RePEc:eee:renene:v:173:y:2021:i:c:p:128-140
    DOI: 10.1016/j.renene.2021.03.099
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    References listed on IDEAS

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    1. Zhu, Yunhua & Biddy, Mary J. & Jones, Susanne B. & Elliott, Douglas C. & Schmidt, Andrew J., 2014. "Techno-economic analysis of liquid fuel production from woody biomass via hydrothermal liquefaction (HTL) and upgrading," Applied Energy, Elsevier, vol. 129(C), pages 384-394.
    2. Castello, Daniele & Haider, Muhammad Salman & Rosendahl, Lasse Aistrup, 2019. "Catalytic upgrading of hydrothermal liquefaction biocrudes: Different challenges for different feedstocks," Renewable Energy, Elsevier, vol. 141(C), pages 420-430.
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    1. Ayala-Cortés, Alejandro & Arcelus-Arrillaga, Pedro & Millan, Marcos & Okoye, Patrick U. & Arancibia-Bulnes, Camilo A. & Pacheco-Catalán, Daniella Esperanza & Villafán-Vidales, Heidi Isabel, 2022. "Solar hydrothermal processing of agave bagasse: Insights on the effect of operational parameters," Renewable Energy, Elsevier, vol. 192(C), pages 14-23.

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