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Nitrogen-incorporated boron-doped diamond films for enhanced electrochemical supercapacitor performance

Author

Listed:
  • Suman, Shradha
  • Ficek, Mateusz
  • Sankaran, Kamatchi Jothiramalingam
  • Ryl, Jacek
  • Rakesh, Benadict
  • Gupta, Mukul
  • Sakthivel, Ramasamy
  • Bogdanowicz, Robert

Abstract

The electrochemical (EC) supercapacitor, known for its rapid charging, reliability, and versatile applications, demands optimized electrode characteristics and an understanding of their electrochemical behaviour. Although boron-doped diamond (BDD) holds promise as a supercapacitor electrode, a crucial gap exists in comprehending its material behaviour under specific growth conditions. Here, nitrogen-incorporated BDD (N-BDD) films with different microstructures are investigated. The morphology of N-BDD films is varied by tuning the substrate temperature (Ts) from 400 °C to 850 °C during the growth process. The diamond films grown at lower Ts = 400 °C consist of faceted grains, and the grain sizes shrink as Ts is increased (550 °C and 700 °C). Interestingly, the films grown at 850 °C (N-BDD850°C) show nanowire-like morphology with enhanced electrical conductivity. The spectroscopy and microscopy results reveal the concurrence of sp3-diamond and sp2-graphitic phases in the nanowire morphology. The EC supercapacitor studies disclose that formation of nanowire-like morphology for N-BDD850°C increases the active surface area and electron transport properties; hence, higher current response and enhanced specific capacitance (0.09 F cm−2 at a current density of 1.53 mA cm−2) are observed. Lifecycle stability of 82% is observed after 5000 cycles indicating the efficient performance of N-BDD850°C films.

Suggested Citation

  • Suman, Shradha & Ficek, Mateusz & Sankaran, Kamatchi Jothiramalingam & Ryl, Jacek & Rakesh, Benadict & Gupta, Mukul & Sakthivel, Ramasamy & Bogdanowicz, Robert, 2024. "Nitrogen-incorporated boron-doped diamond films for enhanced electrochemical supercapacitor performance," Energy, Elsevier, vol. 294(C).
    • Handle: RePEc:eee:energy:v:294:y:2024:i:c:s0360544224006868
    DOI: 10.1016/j.energy.2024.130914
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    References listed on IDEAS

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    1. Olabi, Abdul Ghani & Abbas, Qaisar & Al Makky, Ahmed & Abdelkareem, Mohammad Ali, 2022. "Supercapacitors as next generation energy storage devices: Properties and applications," Energy, Elsevier, vol. 248(C).
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