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A novel approach for preparing in-situ nitrogen doped carbon via pyrolysis of bean pulp for supercapacitors

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  • Ding, Yan
  • Li, Yunchao
  • Dai, Yujie
  • Han, Xinhong
  • Xing, Bo
  • Zhu, Lingjun
  • Qiu, Kunzan
  • Wang, Shurong

Abstract

The preparation of activated carbon by complex and expensive nitrogen doping and activation process has been studied extensively. N-doped activated biochar or carbon material prepared from renewable and low-cost biomass has arisen more and more attention due to the hierarchical porous structure and abundant nitrogenous functional groups in the application of supercapacitors. Herein, a method for preparation of in-situ nitrogen doped activated carbon derived from bean pulp (BPC) by one-step carbonization and CO2 activation at 1073 K was proposed. The morphological structure, specific surface area (SSA), pore size and nitrogen-containing functional group compounds could be controlled by the adjustment of CO2 concentration. The maximum SSA could be up to 558.2 m2 g−1 for BPC. The N content increased from 5.0% to 10.0% with the increase of CO2 concentration from 0 to 50 vol%. In addition, pyridine, pyrrole, graphite, and nitrous oxide were detected and analyzed, in which pyridine and pyrrole nitrogen enhance the pseudocapacitance. A maximum specific capacitance of BPC-50 reached 106 F g−1 at 0.25 A g−1. The capacitance retention maintained 93% at 10 A g−1 after 20,000 cycles in the symmetrical supercapacitor with a 6 M KOH electrolyte.

Suggested Citation

  • Ding, Yan & Li, Yunchao & Dai, Yujie & Han, Xinhong & Xing, Bo & Zhu, Lingjun & Qiu, Kunzan & Wang, Shurong, 2021. "A novel approach for preparing in-situ nitrogen doped carbon via pyrolysis of bean pulp for supercapacitors," Energy, Elsevier, vol. 216(C).
  • Handle: RePEc:eee:energy:v:216:y:2021:i:c:s0360544220323343
    DOI: 10.1016/j.energy.2020.119227
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    References listed on IDEAS

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    1. Zhan, Hao & Zhuang, Xiuzheng & Song, Yanpei & Yin, Xiuli & Wu, Chuangzhi, 2018. "Insights into the evolution of fuel-N to NOx precursors during pyrolysis of N-rich nonlignocellulosic biomass," Applied Energy, Elsevier, vol. 219(C), pages 20-33.
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    1. Muhammad Yaseen & Muhammad Arif Khan Khattak & Muhammad Humayun & Muhammad Usman & Syed Shaheen Shah & Shaista Bibi & Bakhtiar Syed Ul Hasnain & Shah Masood Ahmad & Abbas Khan & Nasrullah Shah & Asif , 2021. "A Review of Supercapacitors: Materials Design, Modification, and Applications," Energies, MDPI, vol. 14(22), pages 1-40, November.
    2. Suman, Shradha & Ficek, Mateusz & Sankaran, Kamatchi Jothiramalingam & Ryl, Jacek & Rakesh, Benadict & Gupta, Mukul & Sakthivel, Ramasamy & Bogdanowicz, Robert, 2024. "Nitrogen-incorporated boron-doped diamond films for enhanced electrochemical supercapacitor performance," Energy, Elsevier, vol. 294(C).
    3. Sun, Bingkang & Zhang, Xiaoyun & Fan, Xing & Wang, Ruiyu & Bai, Hongcun & Wei, Xianyong, 2022. "Interface modification based on MnO2@N-doped activated carbon composites for flexible solid-state asymmetric supercapacitors," Energy, Elsevier, vol. 249(C).
    4. Ozpinar, Pelin & Dogan, Ceren & Demiral, Hakan & Morali, Ugur & Erol, Salim & Samdan, Canan & Yildiz, Derya & Demiral, Ilknur, 2022. "Activated carbons prepared from hazelnut shell waste by phosphoric acid activation for supercapacitor electrode applications and comprehensive electrochemical analysis," Renewable Energy, Elsevier, vol. 189(C), pages 535-548.
    5. Qin, Liyuan & Wu, Yang & Jiang, Enchen, 2022. "In situ template preparation of porous carbon materials that are derived from swine manure and have ordered hierarchical nanopore structures for energy storage," Energy, Elsevier, vol. 242(C).
    6. Olabi, Abdul Ghani & Abbas, Qaisar & Al Makky, Ahmed & Abdelkareem, Mohammad Ali, 2022. "Supercapacitors as next generation energy storage devices: Properties and applications," Energy, Elsevier, vol. 248(C).
    7. Sakthivel, Mani & Ramki, Settu & Chen, Shen-Ming & Ho, Kuo-Chuan, 2022. "Defect rich Se–CoWS2 as anode and banana flower skin-derived activated carbon channels with interconnected porous structure as cathode materials for asymmetric supercapacitor application," Energy, Elsevier, vol. 257(C).

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