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Preparation and solar thermochemical properties analysis of NiFe2O4@SiC/ @Si3N4 for high-performance CO2-splitting

Author

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  • Jiang, Boshu
  • Guene Lougou, Bachirou
  • Zhang, Hao
  • Geng, Boxi
  • Wu, Lianxuan
  • Shuai, Yong

Abstract

The solar-driven thermochemical CO2-to-CO conversion is an effective way to achieve the mission of carbon peaking and carbon neutrality. However, synthesizing porous reacting materials with excellent thermal stability, hardness and long-term cyclic stability, oxygen exchange capacity, and higher CO2-to-CO conversion are the most important challenges associated with the thermochemical CO2-splitting approach and technological upscaling to large-scale applications. This study presented the development of NiFe2O4 oxygen carriers, the synthesis method of SiC and Si3N4 supports, and solar-to-fuel processing of the newly prepared materials through CO2-splitting under a highly concentrated solar radiative heat flux. The newly synthesized NiFe2O4@SiC porous redox material resulted in higher solar energy absorption and CO2 conversion capability with an instantaneous CO production of 410 μmol/g and direct CO2-to-CO conversion rate of 18.1 % at 1073–1273 K reaction temperature. The media composite of NiFe2O4@SiC exhibited high-temperature thermal changes, good thermochemical reaction stability, and a higher CO production rate through six redox cycles compared to NiFe2O4@Si3N4 porous reacting material. The high oxidation potential and remarkably solar radiative heat flux absorption and thermochemical CO2-splitting capacities of the newly developed materials were demonstrated through experimental analysis. The synergistic effect of the oxygen carriers (NiFe2O4) and substrate materials including SiC and Si3N4 skeletons for CO2-splitting is highlighted. This study provided comprehensive and novel experimental insights that can be used as guidance for theoretical research and application in CO2 conversion into high-value-added energy products.

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  • Jiang, Boshu & Guene Lougou, Bachirou & Zhang, Hao & Geng, Boxi & Wu, Lianxuan & Shuai, Yong, 2022. "Preparation and solar thermochemical properties analysis of NiFe2O4@SiC/ @Si3N4 for high-performance CO2-splitting," Applied Energy, Elsevier, vol. 328(C).
    • Handle: RePEc:eee:appene:v:328:y:2022:i:c:s0306261922013149
    DOI: 10.1016/j.apenergy.2022.120057
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    1. Guo, Yongpeng & Chen, Jing & Song, Hualong & Zheng, Ke & Wang, Jian & Wang, Hongsheng & Kong, Hui, 2024. "A review of solar thermochemical cycles for fuel production," Applied Energy, Elsevier, vol. 357(C).
    2. Guene Lougou, Bachirou & Wu, Lianxuan & Ma, Danni & Geng, Boxi & Jiang, Boshu & Han, Donmei & Zhang, Hao & Łapka, Piotr & Shuai, Yong, 2023. "Efficient conversion of solar energy through a macroporous ceramic receiver coupling heat transfer and thermochemical reactions," Energy, Elsevier, vol. 271(C).

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