IDEAS home Printed from https://ideas.repec.org/a/gam/jeners/v12y2019i24p4791-d298494.html
   My bibliography  Save this article

Optimization of Programmed Temperature Vaporization Injection for Determination of Polycyclic Aromatic Hydrocarbons from Diesel Combustion Process

Author

Listed:
  • Yuehan Qiao

    (State Key Laboratory of Engines, Tianjin University, Tianjin 300072, China)

  • Gang Lyu

    (State Key Laboratory of Engines, Tianjin University, Tianjin 300072, China)

  • Chonglin Song

    (State Key Laboratory of Engines, Tianjin University, Tianjin 300072, China)

  • Xingyu Liang

    (State Key Laboratory of Engines, Tianjin University, Tianjin 300072, China)

  • Huawei Zhang

    (School of Mechanical Engineering, North China University of Water Resources and Electric Power, Zhengzhou 450045, China)

  • Dong Dong

    (Institute of High Energy Physics Chinese Academy of Science, Beijing 100049, China)

Abstract

In this study, programmed temperature vaporization in the solvent vent mode (PTV-SV) of gas chromatography-mass spectrometry was optimized and validated for the analysis of particle-phase and gas-phase polycyclic aromatic hydrocarbons from diesel engine combustion. Because of the large number of experimental and response variables to be studied, central composite inscribed design was used to optimize the PTV-SV injection factors, including initial inlet temperature, vaporization flow and time. The optimized PTV-SV method was validated by linearity, accuracy and sensitivity. For the 16 Polycyclic aromatic hydrocarbons (PAHs) studied, the correlation coefficients for the calibration plots of peak areas versus concentrations (0.5–300 ng mL −1 ) ranged from 0.9812–0.9998. Limits of detection ranged from 0.016–20,130.375 ng mL −1 , and limits of quantification ranged from 0.055–1.25 ng mL −1 . The optimized method was used for the analysis of real samples collected from a diesel engine, which included particle-phase and gas-phase PAHs. The results showed that the improved PTV-SV method was satisfying for simultaneously identifying and quantifying PAHs produced during diesel combustion.

Suggested Citation

  • Yuehan Qiao & Gang Lyu & Chonglin Song & Xingyu Liang & Huawei Zhang & Dong Dong, 2019. "Optimization of Programmed Temperature Vaporization Injection for Determination of Polycyclic Aromatic Hydrocarbons from Diesel Combustion Process," Energies, MDPI, vol. 12(24), pages 1-13, December.
    • Handle: RePEc:gam:jeners:v:12:y:2019:i:24:p:4791-:d:298494
    as

    Download full text from publisher

    File URL: https://www.mdpi.com/1996-1073/12/24/4791/pdf
    Download Restriction: no
    File URL: https://www.mdpi.com/1996-1073/12/24/4791/
    Download Restriction: no
    ---><---

    References listed on IDEAS

    as
    1. Yaoyao Ying & Chenxuan Xu & Dong Liu & Bo Jiang & Pengfei Wang & Wei Wang, 2017. "Nanostructure and Oxidation Reactivity of Nascent Soot Particles in Ethylene/Pentanol Flames," Energies, MDPI, vol. 10(1), pages 1-16, January.
    2. Hamisu Adamu Dandajeh & Midhat Talibi & Nicos Ladommatos & Paul Hellier, 2019. "Influence of Combustion Characteristics and Fuel Composition on Exhaust PAHs in a Compression Ignition Engine," Energies, MDPI, vol. 12(13), pages 1-19, July.
    Full references (including those not matched with items on IDEAS)

    Citations

    Citations are extracted by the CitEc Project, subscribe to its RSS feed for this item.
    as


    Cited by:

    1. Yi Dong & Jianmin Liu & Yanbin Liu & Xinyong Qiao & Xiaoming Zhang & Ying Jin & Shaoliang Zhang & Tianqi Wang & Qi Kang, 2020. "A RBFNN & GACMOO-Based Working State Optimization Control Study on Heavy-Duty Diesel Engine Working in Plateau Environment," Energies, MDPI, vol. 13(1), pages 1-24, January.

    Most related items

    These are the items that most often cite the same works as this one and are cited by the same works as this one.
    1. Duan, Jiaqi & Ying, Yaoyao & Liu, Dong, 2019. "Novel nanoscale control on soot formation by local CO2 micro-injection in ethylene inverse diffusion flames," Energy, Elsevier, vol. 179(C), pages 697-708.
    2. Bo Jiang & Pengfei Wang & Yaoyao Ying & Minye Luo & Dong Liu, 2018. "Nanoscale Characteristics and Reactivity of Nascent Soot from n -Heptane/2,5-Dimethylfuran Inverse Diffusion Flames with/without Magnetic Fields," Energies, MDPI, vol. 11(7), pages 1-21, July.
    3. Wei Wang & Dong Liu & Yaoyao Ying & Guannan Liu & Ye Wu, 2017. "On the Response of Nascent Soot Nanostructure and Oxidative Reactivity to Photoflash Exposure," Energies, MDPI, vol. 10(7), pages 1-11, July.
    4. Nadir Yilmaz & Francisco M. Vigil & Alpaslan Atmanli & Burl Donaldson, 2022. "Detailed Analysis of PAH Formation, Toxicity and Regulated Pollutants in a Diesel Engine Running on Diesel Blends with n-Propanol, n-Butanol and n-Pentanol," Energies, MDPI, vol. 15(17), pages 1-14, September.
    5. Luo, Minye & Liu, Dong, 2018. "Effects of dimethyl ether addition on soot formation, evolution and characteristics in flame-wall interactions," Energy, Elsevier, vol. 164(C), pages 642-654.
    6. Cabrera-Jiménez, Richard & Mateo-Sanz, Josep M. & Gavaldà, Jordi & Jiménez, Laureano & Pozo, Carlos, 2022. "Comparing biofuels through the lens of sustainability: A data envelopment analysis approach," Applied Energy, Elsevier, vol. 307(C).

    Corrections

    All material on this site has been provided by the respective publishers and authors. You can help correct errors and omissions. When requesting a correction, please mention this item's handle: RePEc:gam:jeners:v:12:y:2019:i:24:p:4791-:d:298494. See general information about how to correct material in RePEc.

    If you have authored this item and are not yet registered with RePEc, we encourage you to do it here. This allows to link your profile to this item. It also allows you to accept potential citations to this item that we are uncertain about.

    If CitEc recognized a bibliographic reference but did not link an item in RePEc to it, you can help with this form .

    If you know of missing items citing this one, you can help us creating those links by adding the relevant references in the same way as above, for each refering item. If you are a registered author of this item, you may also want to check the "citations" tab in your RePEc Author Service profile, as there may be some citations waiting for confirmation.

    For technical questions regarding this item, or to correct its authors, title, abstract, bibliographic or download information, contact: MDPI Indexing Manager (email available below). General contact details of provider: https://www.mdpi.com .

    Please note that corrections may take a couple of weeks to filter through the various RePEc services.

    IDEAS is a RePEc service. RePEc uses bibliographic data supplied by the respective publishers.