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Unveiling one-pot scalable fabrication of reusable carboxylated heterogeneous carbon-based catalysts from eucalyptus plant with the assistance of dry ice for selective hydrolysis of eucalyptus biomass

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  • Abdu, Hassan Idris
  • Eid, Kamel
  • Abdullah, Aboubakr M.
  • Han, Zhengang
  • Ibrahim, Mohammed Hassan
  • Shan, Duoliang
  • Chen, Jing
  • Elzatahry, Ahmed A.
  • Lu, Xiaoquan

Abstract

Biomass is the most abundant source for organic carbon-based substances on the earth; however, its utilization as sources for heterogeneous catalysts for biorefineries is rarely reported. Herein, a simple approach was developed for tailoring one-pot fabrication of carboxylate heterogeneous catalysts from woody biomass eucalyptus denoted as (ECS) via the ball-milling in the presence of dry ice as an oxidant followed by protonation. The ECS catalyst was obtained in a high yield of (100%) without any waste, organic solvents, and multistep reactions. The resultant ECS is composed of an aromatic skeleton enriched with a carboxylic group (COOH) of (2.4 mmol g−1) as well as some aliphatic moieties (CH0.44O0.42). The COOH content in the ECS was a function of the ball-milling time. The newly designed ECS catalyst allowed the successful hydrolysis of eucalyptus biomass to xylose (95.1%) and glucose (81%) at 180 °C within only 17 min in the presence of 120 ppm of HCl. Intriguingly, the obtained solid residuals of both catalysts and unhydrolyzed eucalyptus could be milled again to form a fresh ECS catalyst. The presented approach opens new avenues for the fabrication of scalable heterogeneous-carbon catalysts for biorefineries applications.

Suggested Citation

  • Abdu, Hassan Idris & Eid, Kamel & Abdullah, Aboubakr M. & Han, Zhengang & Ibrahim, Mohammed Hassan & Shan, Duoliang & Chen, Jing & Elzatahry, Ahmed A. & Lu, Xiaoquan, 2020. "Unveiling one-pot scalable fabrication of reusable carboxylated heterogeneous carbon-based catalysts from eucalyptus plant with the assistance of dry ice for selective hydrolysis of eucalyptus biomass," Renewable Energy, Elsevier, vol. 153(C), pages 998-1004.
    • Handle: RePEc:eee:renene:v:153:y:2020:i:c:p:998-1004
    DOI: 10.1016/j.renene.2020.02.034
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    References listed on IDEAS

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    1. Masakazu Toda & Atsushi Takagaki & Mai Okamura & Junko N. Kondo & Shigenobu Hayashi & Kazunari Domen & Michikazu Hara, 2005. "Biodiesel made with sugar catalyst," Nature, Nature, vol. 438(7065), pages 178-178, November.
    2. Rode, Rafael & Leite, Helio Garcia & Silva, Márcio Lopes da & Ribeiro, Carlos Antonio Álvares Soares & Binoti, Daniel Henrique Breda, 2014. "The economics and optimal management regimes of eucalyptus plantations: A case study of forestry outgrower schemes in Brazil," Forest Policy and Economics, Elsevier, vol. 44(C), pages 26-33.
    3. Gibbins, Jon & Chalmers, Hannah, 2008. "Carbon capture and storage," Energy Policy, Elsevier, vol. 36(12), pages 4317-4322, December.
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