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Preparation of low hydration heat cement slurry with micro-encapsulated thermal control material

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  • Feng, Qian
  • Liu, Xian-jie
  • Peng, Zhi-gang
  • Zheng, Yong
  • Huo, Jin-hua
  • Liu, Huan

Abstract

During the cementing process of natural gas hydrate (NGH) layer, the hydration heat of cement slurry can easily cause decomposition of NGH which leads to cementing risk. A thermal control material of phase change micro-capsule (PCM-1) with paraffin as the core material and urea-formaldehyde resin as the wall material was successfully synthesized, and then a low hydration heat cement slurry was prepared by using PCM-1. The basic performances of PCM-1 were characterized by using DSC, FTIR, SEM and TG, and the results show that the performances meet designed requirements. Then, the PCM-1 was introduced into cement slurry system, and the hydration heat (Q) and hydration temperature rise (Tr) were measured by using the self-developed semi-adiabatic test equipment. As a result, it was confirmed that the Q and the Tr decrease with the increase of PCM-1 content. The Tr of cement slurry CP15% was 25.4 °C, lower than that of cement slurry CB. Meanwhile, compared with cement slurry CB, at 24 and 48 h hydration heat of cement slurry CP15% were decreased by 7.68 × 104 and 7.28 × 104 J, respectively. Therefore, the decomposition of NGH was avoided attribute to the smaller Q of cement slurry, and the cementing operation risk in deep water was reduced.

Suggested Citation

  • Feng, Qian & Liu, Xian-jie & Peng, Zhi-gang & Zheng, Yong & Huo, Jin-hua & Liu, Huan, 2019. "Preparation of low hydration heat cement slurry with micro-encapsulated thermal control material," Energy, Elsevier, vol. 187(C).
    • Handle: RePEc:eee:energy:v:187:y:2019:i:c:s0360544219316949
    DOI: 10.1016/j.energy.2019.116000
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    References listed on IDEAS

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    Cited by:

    1. Huo, Jinhua & Zhang, Ruizhi & Yu, Baisong & Che, Yuanjun & Wu, Zhansheng & Zhang, Xing & Peng, Zhigang, 2022. "Preparation, characterization, investigation of phase change micro-encapsulated thermal control material used for energy storage and temperature regulation in deep-water oil and gas development," Energy, Elsevier, vol. 239(PD).
    2. Emiliano Borri & Nan Hua & Adriano Sciacovelli & Dawei Wu & Yulong Ding & Yongliang Li & Vincenza Brancato & Yannan Zhang & Andrea Frazzica & Wenguang Li & Zhibin Yu & Yanio E. Milian & Svetlana Ushak, 2022. "Phase Change Slurries for Cooling and Storage: An Overview of Research Trends and Gaps," Energies, MDPI, vol. 15(19), pages 1-17, September.
    3. Ren, Miao & Zhao, Hua & Gao, Xiaojian, 2022. "Effect of modified diatomite based shape-stabilized phase change materials on multiphysics characteristics of thermal storage mortar," Energy, Elsevier, vol. 241(C).
    4. Ran, Fengming & Xu, Changlu & Chen, Yunkang & Cong, Rongshuai & Fang, Guiyin, 2021. "Numerical flow characteristics of microencapsulated phase change slurry flowing in a helically coiled tube for thermal energy storage," Energy, Elsevier, vol. 223(C).

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