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Conversion of fructose to 5-hydroxymethylfurfural using solution plasma process

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  • Klanarong, Nattha
  • Saito, Nagahiro
  • Prasertsung, Isarawut
  • Damrongsakkul, Siriporn

Abstract

5-hydroxymethylfurfural (HMF), a key building block chemical derived from renewable lignocellulosic biomass, is used to produce a variety of derivatives for the biorefinery industry. In this work, the solution plasma process (SPP) was first applied to convert fructose, a key component from biomass, into HMF. Various conditions that affect fructose conversion and HMF yield were studied, including plasma treatment time (0–300 min), DMSO concentration (0–70%), electrode types (Iron; Fe and tungsten; W), system temperature (70–90 °C) and initial fructose concentration (10 g/L and 25 g/L). SPP was showed to enhance the conversion process to achieve high fructose conversion and HMF yield at the temperature (90 °C) lower than other conventional heating processes. The maximum fructose conversion and HMF yield were achieved at 95% and 76%, respectively at the DMSO concentration of 70% with Fe-electrodes, 90 °C of system temperature, 10 g/L of initial fructose concentration, 22.5 kHz of pulsed frequency and plasma treatment time of 240 min. Sulfuric acid formed from DMSO dissociation and Fe-nanoparticles from electrode erosion could effectively act as catalysts for the dehydration of fructose to HMF. SPP can be a high-potential tool for enhancing HMF production from the dehydration process in BCG economy.

Suggested Citation

  • Klanarong, Nattha & Saito, Nagahiro & Prasertsung, Isarawut & Damrongsakkul, Siriporn, 2023. "Conversion of fructose to 5-hydroxymethylfurfural using solution plasma process," Renewable Energy, Elsevier, vol. 218(C).
    • Handle: RePEc:eee:renene:v:218:y:2023:i:c:s0960148123012144
    DOI: 10.1016/j.renene.2023.119299
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    References listed on IDEAS

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    1. Dowaki, Taishi & Guo, Haixin & Smith, Richard Lee, 2022. "Lignin-derived biochar solid acid catalyst for fructose conversion into 5-ethoxymethylfurfural," Renewable Energy, Elsevier, vol. 199(C), pages 1534-1542.
    2. Wang, Shuai & Eberhardt, Thomas L. & Guo, Dayi & Feng, Junfeng & Pan, Hui, 2022. "Efficient conversion of glucose into 5-HMF catalyzed by lignin-derived mesoporous carbon solid acid in a biphasic system," Renewable Energy, Elsevier, vol. 190(C), pages 1-10.
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    1. Yin, Kexin & Wang, Yangyang & Wu, Qiming & Zhang, Jifu & Zhou, Yaru & Xu, Zaifeng & Zhu, Zhaoyou & Qi, Jianguang & Wang, Yinglong & Cui, Peizhe, 2024. "Thermodynamic analysis of a plasma co-gasification process for hydrogen production using sludge and food waste as mixed raw materials," Renewable Energy, Elsevier, vol. 222(C).

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