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A novel upscaling procedure for characterising heterogeneous shale porosity from nanometer-to millimetre-scale in 3D

Author

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  • Ma, Lin
  • Dowey, Patrick J.
  • Rutter, Ernest
  • Taylor, Kevin G.
  • Lee, Peter D.

Abstract

Microstructures and pore systems in shales are key to understanding the role of shale in many energy applications. This study proposes a novel multi-stage upscaling procedure to comprehensively investigate the heterogeneous and complex microstructures and pore systems in a laminated and microfractured shale, utilising 3D multi-scale imaging data. Five imaging techniques were used for characterisation from sub-nanoscale to macroscale (core-scale), spanning four orders of magnitude. Image data collected using X-ray tomography, Focused Ion Beam, and Electron Tomography techniques range in voxel size from 0.6 nm to 13 μm.

Suggested Citation

  • Ma, Lin & Dowey, Patrick J. & Rutter, Ernest & Taylor, Kevin G. & Lee, Peter D., 2019. "A novel upscaling procedure for characterising heterogeneous shale porosity from nanometer-to millimetre-scale in 3D," Energy, Elsevier, vol. 181(C), pages 1285-1297.
    • Handle: RePEc:eee:energy:v:181:y:2019:i:c:p:1285-1297
    DOI: 10.1016/j.energy.2019.06.011
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    Citations

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    Cited by:

    1. Wei, Jianguang & Li, Jiangtao & Zhang, Ao & Shang, Demiao & Zhou, Xiaofeng & Niu, Yintao, 2023. "Influence of shale bedding on development of microscale pores and fractures," Energy, Elsevier, vol. 282(C).
    2. Wu, Mingqiu & Li, Haitao & Wang, Liang & Yang, Xinlei & Dai, Chongyang & Yang, Ning & Li, Jie & Wang, Yu & Yu, Minggao, 2023. "μCT quantitative assessment of the pore–fracture structures and permeability behaviors of long-flame coal treated by infrared rapid heating," Energy, Elsevier, vol. 274(C).
    3. Zhu, Hongjian & Ju, Yiwen & Huang, Cheng & Chen, Fangwen & Chen, Bozhen & Yu, Kun, 2020. "Microcosmic gas adsorption mechanism on clay-organic nanocomposites in a marine shale," Energy, Elsevier, vol. 197(C).
    4. Liao, Qinzhuo & Li, Gensheng & Tian, Shouceng & Song, Xianzhi & Lei, Gang & Liu, Xu & Chen, Weiqing & Patil, Shirish, 2023. "An efficient analytical approach for steady-state upscaling of relative permeability and capillary pressure," Energy, Elsevier, vol. 282(C).
    5. Wei, Jianguang & Zhou, Xiaofeng & Shamil, Sultanov & Yuriy, Kotenev & Yang, Erlong & Yang, Ying & Wang, Anlun, 2023. "Lithofacies influence characteristics on typical shale pore structure," Energy, Elsevier, vol. 282(C).
    6. Medina, Federico Javier & Jausoro, Ignacio & Floridia Addato, María Alejandra & Rodriguez, María Jimena & Tomassini, Federico González & Caneiro, Alberto, 2022. "On the evaluation of Representative Elementary Area for porosity in shale rocks by Field Emission Scanning Electron Microscopy," Energy, Elsevier, vol. 253(C).
    7. Li, Jiangtao & Zhou, Xiaofeng & Liu, Xibao & Gayubov, Abdumalik & Shamil, Sultanov, 2023. "Cross-scale diffusion characteristics in microscale fractures of tight and shale gas reservoirs considering real gas – mixture – body diffusion – water film coupling," Energy, Elsevier, vol. 283(C).
    8. Ma, Lin & Fauchille, Anne-Laure & Chandler, Michael R. & Dowey, Patrick & Taylor, Kevin G. & Mecklenburgh, Julian & Lee, Peter D., 2021. "In-situ synchrotron characterisation of fracture initiation and propagation in shales during indentation," Energy, Elsevier, vol. 215(PB).
    9. Zhou, H.W. & Liu, Z.L. & Zhong, J.C. & Chen, B.C. & Zhao, J.W. & Xue, D.J., 2022. "NMRI online observation of coal fracture and pore structure evolution under confining pressure and axial compressive loads: A novel approach," Energy, Elsevier, vol. 261(PA).
    10. Zhou, Zhixiang & Wen, Hang & Pang, Huiwen & Liang, Lihao & Jiang, Xingwen & Song, Jiabang, 2024. "Energy evolution analysis of heat-treated hydrated shale," Energy, Elsevier, vol. 289(C).
    11. Rezaeyan, Amirsaman & Kampman, Niko & Pipich, Vitaliy & Barnsley, Lester C. & Rother, Gernot & Magill, Clayton & Ma, Jingsheng & Busch, Andreas, 2024. "Compaction and clay content control mudrock porosity," Energy, Elsevier, vol. 289(C).
    12. Shi, Rui & Liu, Jishan & Wang, Xiaoming & Wei, Mingyao & Elsworth, Derek, 2021. "A critical analysis of shale laboratory permeability evolution data," Energy, Elsevier, vol. 236(C).
    13. Nie, Bin, 2023. "Diffusion characteristics of shale mixed gases on the wall of microscale fractures," Energy, Elsevier, vol. 284(C).
    14. Cao, Gaohui & Jiang, Wenbin & Lin, Mian & Ji, Lili & Xu, Zhipeng & Zheng, Siping & Hao, Fang, 2021. "Mortar dynamic coupled model for calculating interface gas exchange between organic and inorganic matters of shale," Energy, Elsevier, vol. 236(C).
    15. Zeng, Fang & Dong, Chunmei & Lin, Chengyan & Tian, Shansi & Wu, Yuqi & Lin, Jianli & Liu, Binbin & Zhang, Xianguo, 2022. "Pore structure characteristics of reservoirs of Xihu Sag in East China Sea Shelf Basin based on dual resolution X-ray computed tomography and their influence on permeability," Energy, Elsevier, vol. 239(PD).

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