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Photocatalytic hydrogen evolution from water splitting using Cu doped ZnS microspheres under visible light irradiation

Author

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  • Lee, Gang-Juan
  • Anandan, Sambandam
  • Masten, Susan J.
  • Wu, Jerry J.

Abstract

Cu/ZnS microspheres have been successfully synthesized using microwave irradiation method without using any template. Cu/ZnS microspheres were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), high resolution transmission electron microscopy (HR-TEM), inductively coupled plasma optima optical emission spectrometer (ICP-OES), X-ray photoelectron spectroscopy (XPS), diffused reflectance spectroscopy (DRS), and electrochemical impedance spectroscopy (EIS) methods. Tuning of band gap from 3.43 to 2.36 eV was successfully achieved upon doping copper (0–10%) into ZnS. The photocatalytic activity was investigated by photosplitting of water containing an aqueous Na2S solution under visible light irradiation. Among the prepared photocatalysts, the hydrogen evolution rate reaches the maximum of about 973.1 μmol h−1 g−1 for 2.0 mol% Cu2+ ion doped ZnS. Moreover, Cu/ZnS microspheres were found photocatalytically stable during the 48 h test runs.

Suggested Citation

  • Lee, Gang-Juan & Anandan, Sambandam & Masten, Susan J. & Wu, Jerry J., 2016. "Photocatalytic hydrogen evolution from water splitting using Cu doped ZnS microspheres under visible light irradiation," Renewable Energy, Elsevier, vol. 89(C), pages 18-26.
    • Handle: RePEc:eee:renene:v:89:y:2016:i:c:p:18-26
    DOI: 10.1016/j.renene.2015.11.083
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    Cited by:

    1. Zhao, Wan & Chen, Zhi & Yang, Xiuru & Qian, Xiaoxiao & Liu, Chunxi & Zhou, Dantong & Sun, Tao & Zhang, Ming & Wei, Guoying & Dissanayake, Pavani Dulanja & Ok, Yong Sik, 2020. "Recent advances in photocatalytic hydrogen evolution with high-performance catalysts without precious metals," Renewable and Sustainable Energy Reviews, Elsevier, vol. 132(C).
    2. Raheman AR, Shakeelur & Wilson, Higgins M. & Momin, Bilal M. & Annapure, Uday S. & Jha, Neetu, 2020. "CdSe quantum dots modified thiol functionalized g-C3N4: Intimate interfacial charge transfer between 0D/2D nanostructure for visible light H2 evolution," Renewable Energy, Elsevier, vol. 158(C), pages 431-443.
    3. Tang, Liang & Wang, Jing & Liu, Xudong & Shu, Xiaoqing & Zhang, Zhaohong & Wang, Jun, 2019. "Fabrication of Z-scheme photocatalyst, Er3+:Y3Al5O12@NiGa2O4-MWCNTs-WO3, and visible-light photocatalytic activity for degradation of organic pollutant with simultaneous hydrogen evolution," Renewable Energy, Elsevier, vol. 138(C), pages 474-488.
    4. Saraswat, Sushil Kumar & Rodene, Dylan D. & Gupta, Ram B., 2018. "Recent advancements in semiconductor materials for photoelectrochemical water splitting for hydrogen production using visible light," Renewable and Sustainable Energy Reviews, Elsevier, vol. 89(C), pages 228-248.
    5. Fang, Wei & Zhao, Lei & He, Xuan & Chen, Hui & Li, Weixin & Zeng, Xianghui & Chen, Xiaodong & Shen, Yue & Zhang, Wenhao, 2020. "Carbonized rice husk foam constructed by surfactant foaming method for solar steam generation," Renewable Energy, Elsevier, vol. 151(C), pages 1067-1075.
    6. Aguilar-Martínez, Octavio & Hernández-Gordillo, Agileo & Pérez-Hernández, Raúl & Acevedo-Peña, Próspero & Arrieta-Castañeda, Alma & Gómez, Ricardo & Tzompantzi, Francisco, 2017. "Efficient ZnO1-xSx composites from the Zn5(CO3)2(OH)6 precursor for the H2 production by photocatalysis," Renewable Energy, Elsevier, vol. 113(C), pages 43-51.
    7. Bashiri, Robabeh & Mohamed, Norani Muti & Kait, Chong Fai & Sufian, Suriati & Kakooei, Saied & Khatani, Mehboob & Gholami, Zahra, 2016. "Optimization hydrogen production over visible light-driven titania-supported bimetallic photocatalyst from water photosplitting in tandem photoelectrochemical cell," Renewable Energy, Elsevier, vol. 99(C), pages 960-970.

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