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Ynthesis and Characterization of Nonstructural MG2NI with Replacement Diffusion Method

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  • Yanqiu Jin
  • Xiuyun Yang
  • Yunhui Li
  • Wenjuan Zhang
  • Limin Wang
  • Yaoming Wu

Abstract

Nonstructural Mg2Ni powder was prepared by replacement-diffusion method. The structure of the Mg2Ni powder was investigated by X-ray diffraction and transmission electron microscopy. Crystallographic structure analysis showed that the synthesized sample powder was constituted with Mg2Ni and a small fraction of MgO. The TEM image in low-resolution indicated that the diameter of the synthesized Mg2Ni powder was in the range of 20~80 nm, and the high-resolution transmission electron microscope (HRTEM) image suggested that the interlinear spacing of (113) lattice planes was 0.229 nm, and the specific surface area examined was 50 m2 /g. The electrochemical hydrogen storage capacity of the Mg2Ni power was also measured in this work. It was 82.5 mAh g-1. The reasons of the low capacity hydrogen storage and decrepitating were analyzed, and the mainly cause were the grievous oxidation of the powder and the pulverization.

Suggested Citation

  • Yanqiu Jin & Xiuyun Yang & Yunhui Li & Wenjuan Zhang & Limin Wang & Yaoming Wu, 2010. "Ynthesis and Characterization of Nonstructural MG2NI with Replacement Diffusion Method," Modern Applied Science, Canadian Center of Science and Education, vol. 4(8), pages 114-114, August.
    • Handle: RePEc:ibn:masjnl:v:4:y:2010:i:8:p:114
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    References listed on IDEAS

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    JEL classification:

    • R00 - Urban, Rural, Regional, Real Estate, and Transportation Economics - - General - - - General
    • Z0 - Other Special Topics - - General

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